Sulfamic acid, 1,2-cyclohexanediyl ester

Base Information

• Chemical Name: Sulfamic acid, 1,2-cyclohexanediyl ester
• CAS No.: 77658-11-8
• Molecular Formula: C₆H₁₄N₂O₆S₂
• Molecular Weight: 274.319
• Hs Code.: 2935009090
• DSSTox Substance ID: DTXSID80998870
• ChEMBL ID: CHEMBL170478
• Mol file: 77658-11-8.mol

Synonyms:77658-11-8;Sulfamic acid, 1,2-cyclohexanediyl ester;CHEMBL170478;cyclohexane-1,2-diyl disulfamate;DTXSID80998870

Chemical Property of Sulfamic acid, 1,2-cyclohexanediyl ester

Chemical Property:

• Vapor Pressure: 2.63E-09mmHg at 25°C
• Boiling Point: 478.2°C at 760 mmHg
• Flash Point: 243°C
• PSA: 155.54000
• Density: 1.6g/cm³
• LogP: 2.30000
• XLogP3: -0.9
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 4
• Exact Mass: 274.02932852
• Heavy Atom Count: 16
• Complexity: 377

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(C(C1)OS(=O)(=O)N)OS(=O)(=O)N

Technology Process of Sulfamic acid, 1,2-cyclohexanediyl ester

There total 1 articles about Sulfamic acid, 1,2-cyclohexanediyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-Cyclohexanediol (931-17-9) → Sulfamic acid 2-sulfamoyloxy-cyclohexyl ester (77658-11-8)

Guidance literature:

With sulphamoyl chloride; sodium hydride; Yield given. Multistep reaction; 1.) 1,2-dimethoxyethane, RT, 2 h, 2.) 1,2-dimethoxyethane, 4 deg C, 24 h;

DOI:10.1021/jm00139a029

upstream raw materials:

1,2-Cyclohexanediol

Refernces