(2E)-2-hydroxyimino-3,4-dihydronaphthalen-1-one

Base Information

Chemical Name:(2E)-2-hydroxyimino-3,4-dihydronaphthalen-1-one
CAS No.:39262-02-7
Molecular Formula:C10H9NO2
Molecular Weight:175.187
Hs Code.:
NSC Number:107359
DSSTox Substance ID:DTXSID40423456
Mol file:39262-02-7.mol

Synonyms:MLS002703967;39262-02-7;NSC107359;DTXSID40423456;NSC-107359

Suppliers and Price of (2E)-2-hydroxyimino-3,4-dihydronaphthalen-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (2E)-2-hydroxyimino-3,4-dihydronaphthalen-1-one

Chemical Property:

Vapor Pressure:7.71E-06mmHg at 25°C
Boiling Point:360.9°C at 760 mmHg
Flash Point:172.1°C
Density:1.29g/cm³
XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:175.063328530
Heavy Atom Count:13
Complexity:247

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC(=NO)C(=O)C2=CC=CC=C21
Isomeric SMILES:C1C/C(=N\O)/C(=O)C2=CC=CC=C21

Technology Process of (2E)-2-hydroxyimino-3,4-dihydronaphthalen-1-one

There total 1 articles about (2E)-2-hydroxyimino-3,4-dihydronaphthalen-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 110-46-3
isopentyl nitrite

: 39262-02-7
2-hydroxyimino-1,2,3,4-tetrahydronaphthalen-1-one

: isopentyl 2-(3-(hydroxyimino)propyl)benzoate

: isopentyl 2-(3-(hydroxyimino)propyl)benzoate

Guidance literature:: 3,4-dihydronaphthalene-1(2H)-one; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.25h; Inert atmosphere; Schlenk technique;

isopentyl nitrite; In tetrahydrofuran; at -78 - -40 ℃; for 1h; Optical yield = 28.571 percent de; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.joc.1c01169

Reference yield: 79.0%

: 39262-02-7
2-hydroxyimino-1,2,3,4-tetrahydronaphthalen-1-one

: 2-(2-cyanoethyl)benzoyl fluoride

Guidance literature:: With diethylamino-sulfur trifluoride; In dichloromethane; at 20 ℃; for 0.166667h; chemoselective reaction; Inert atmosphere;
DOI:10.1021/acs.orglett.0c02603