3-(Acetylamino)-3-deoxy-1,2-O-(1-methylethylidene)pentofuranose

Base Information

• Chemical Name: 3-(Acetylamino)-3-deoxy-1,2-O-(1-methylethylidene)pentofuranose
• CAS No.: 29881-53-6
• Molecular Formula: C10H17 N O5
• Molecular Weight: 231.249
• NSC Number: 127228
• DSSTox Substance ID: DTXSID80952336
• Mol file: 29881-53-6.mol

Synonyms:3-(Acetylamino)-3-deoxy-1,2-O-(1-methylethylidene)pentofuranose;29881-53-6;NSC 127228;NSC 693926;NSC127228;NSC693926;DTXSID80952336;NGDMCQAAEDAQDO-UHFFFAOYSA-N;NSC-127228;N-[5-(hydroxymethyl)-2,2-dimethyl-3a,5,6,6a-tetrahydrofuro[2,3-d][1,3]dioxol-6-yl]acetamide;3-(Acetylamino)-3-deoxy-1,2-O-(1-methylethylidene)pentofuranose #;3-Acetamido-3-deoxy-1,2-O-isopropylidene .alpha.-d-ribofuranose;3-Deoxy-3-[(1-hydroxyethylidene)amino]-1,2-O-(1-methylethylidene)pentofuranose

Chemical Property of 3-(Acetylamino)-3-deoxy-1,2-O-(1-methylethylidene)pentofuranose

Chemical Property:

• Vapor Pressure: 6.43E-09mmHg at 25°C
• Boiling Point: 422.8°Cat760mmHg
• Flash Point: 209.5°C
• Density: 1.28g/cm³
• XLogP3: -0.4
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 2
• Exact Mass: 231.11067264
• Heavy Atom Count: 16
• Complexity: 293

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1C(OC2C1OC(O2)(C)C)CO

Technology Process of 3-(Acetylamino)-3-deoxy-1,2-O-(1-methylethylidene)pentofuranose

There total 3 articles about 3-(Acetylamino)-3-deoxy-1,2-O-(1-methylethylidene)pentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-amino-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose (14125-95-2) + acetic anhydride (108-24-7) → 3-Acetamino-3-desoxy-1,2-O-isopropyliden-α-D-ribofuranose (29881-53-6)

Guidance literature:

With pyridine; at 20 ℃; for 3h;

DOI:10.1021/ja073992i

Reference yield:

→ 3-Acetamino-3-desoxy-1,2-O-isopropyliden-α-D-ribofuranose (29881-53-6)

Guidance literature:

Allofuranose 1, NaBH4;

DOI:10.1246/bcsj.43.2966

Reference yield:

→ N-((3aR,5R)-5-Hydroxymethyl-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl)-acetamide (29881-53-6,31826-51-4,32778-81-7,34296-94-1)

Guidance literature:

18, 2.) Na-(meta)perjodat, 2.) NaBH4;

DOI:10.1016/S0008-6215(00)81165-9

upstream raw materials:

3-amino-3-deoxy-1,2-O-isopropylidene-α-D-ribofuranose

acetic anhydride

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