4-METHYL-2-P-TOLYLAZO-PHENYLAMINE

Base Information

• Chemical Name: 4-METHYL-2-P-TOLYLAZO-PHENYLAMINE
• CAS No.: 58010-91-6
• Molecular Formula: C14H15 N3
• Molecular Weight: 225.293
• Hs Code.: 2927000090
• Mol file: 58010-91-6.mol

Synonyms:Benzenamine,4-methyl-2-[(4-methylphenyl)azo]- (9CI); p-Toluidine, 2-(p-tolylazo)-(6CI,7CI); 2-(p-Tolylazo)-p-toluidine; 4',5-Dimethyl-2-aminoazobenzene

Chemical Property of 4-METHYL-2-P-TOLYLAZO-PHENYLAMINE

Chemical Property:

• Vapor Pressure: 1.16E-06mmHg at 25°C
• Boiling Point: 401.7°Cat760mmHg
• Flash Point: 196.7°C
• PSA: 50.74000
• Density: 1.09g/cm³
• LogP: 4.88220

Purity/Quality:

98%min ^*data from raw suppliers

4-Methyl-2-[(E)-(4-methylphenyl)diazenyl]aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-METHYL-2-P-TOLYLAZO-PHENYLAMINE

There total 14 articles about 4-METHYL-2-P-TOLYLAZO-PHENYLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

1,3-di(p-tolyl)triaz-1-ene (785-86-4,813445-46-4) → 4-methyl-2-p-tolylazo-aniline (58010-91-6)

Guidance literature:

With hydrogenchloride; In tert-butyl alcohol; at 30 ℃; for 48h;

DOI:10.1246/bcsj.54.2853

Reference yield: 13.0%

N,N-dimethyl-aniline (121-69-7,77733-26-7) + 1,3-di(p-tolyl)triaz-1-ene (785-86-4,813445-46-4) → 4-methyl-2-p-tolylazo-aniline (58010-91-6) + N,N-dimethyl-4-(p-tolyldiazenyl)aniline (3010-57-9)

Guidance literature:

With hydrogenchloride; In ethanol; for 72h;

DOI:10.1246/bcsj.54.2853

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + N-(4,4'-bis-dimethylamino-benzhydrylidene)-4-methyl-2-p-tolylazo-aniline → 4-methyl-2-p-tolylazo-aniline (58010-91-6) + bis(p-dimethylaminophenyl)methanone (90-94-8)

Guidance literature:

upstream raw materials:

1-(p-chlorophenyl)-3-(p-tolyl)-triazene

p-toluidine hydrochloride

p-toluidine

N-cyano-3-p-tolyl-triazene-1-carboxamidine

Downstream raw materials:

1,2,3,4-tetrahydro-7-methylphenazine

acetic acid-(4-methyl-2-p-tolylazo-anilide)

2-ethyl-6-methyl-1-p-toluidino-1H-benzimidazole

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