Anthracene-1,8-diol

Base Information

• Chemical Name: Anthracene-1,8-diol
• CAS No.: 607-61-4
• Molecular Formula: C14H10O2
• Molecular Weight: 210.22800
• Hs Code.: 2907299090
• ChEMBL ID: CHEMBL3277319
• DSSTox Substance ID: DTXSID90599897
• Nikkaji Number: J7.007F
• Wikidata: Q82495860
• Mol file: 607-61-4.mol

Synonyms:ANTHRACENE-1,8-DIOL;607-61-4;1,8-dihydroxyanthracene;SCHEMBL430311;CHEMBL3277319;DTXSID90599897

Chemical Property of Anthracene-1,8-diol

Chemical Property:

• PSA: 40.46000
• LogP: 3.40420
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 210.068079557
• Heavy Atom Count: 16
• Complexity: 229

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=CC3=C(C=C2C(=C1)O)C(=CC=C3)O

Technology Process of Anthracene-1,8-diol

There total 8 articles about Anthracene-1,8-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

anthracene-1,8-disulphonic acid (61736-92-3) → 1,8-dihydroxyanthraquinone (607-61-4)

Guidance literature:

With potassium hydroxide; Heating;

Reference yield: 84.0%

1,8-dimethoxyanthracene (16294-34-1) → 1,8-dihydroxyanthraquinone (607-61-4)

Guidance literature:

With boron tribromide; In dichloromethane;

DOI:10.1016/j.tetlet.2004.06.135

Reference yield:

1,8-diacetoxy-9,10-anthraquinone (1963-82-2) → 1,8-dihydroxy-9,10-dihydroanthracene (64817-82-9) + 1,8-dihydroxyanthraquinone (607-61-4)

Guidance literature:

1,8-diacetoxy-9,10-anthraquinone; With acetic acid; zinc; at 135 ℃;

With pyridine; acetyl chloride; at 0 - 20 ℃;

With methylamine; In methanol; dichloromethane; at 0 - 20 ℃;

DOI:10.1055/s-2008-1078499

upstream raw materials:

anthracene-1,8-disulphonic acid

1,8-dimethoxyanthracene

anthracene

1,8-diacetoxy-9,10-anthraquinone

Downstream raw materials:

1,8-diacetoxyanthracene

Refernces

• 1、 Tang, Bo,Yang, Hong-Mei,Hu, Wen-Jing,Ma, Ming-Liang,Liu, Yahu A.,Li, Jiu-Sheng,Jiang, Biao,Wen, Ke. "1,8-Dioxyanthracene-Derived Crown Ethers: Synthesis, Complexation with Paraquat and Assembly of a Tetracationic Cyclophane-Crown Ether Based [2]Catenane". . p. 6925 - 6934. Retrieved 2016/02/19.
• 2、 Quast, Helmut,Fuchsbauer, Hans-Lothar. "ESR Spectroscopic Detection of Intramolecular Interactions in Radical Cations of Poly(α-methoxy)triptycenes". . p. 1016 - 1038. Retrieved 2007/10/02.