5-Iodobenzofuran

Base Information

• Chemical Name: 5-Iodobenzofuran
• CAS No.: 60770-67-4
• Molecular Formula: C8H5IO
• Molecular Weight: 244.032
• Hs Code.: 2932990090
• Mol file: 60770-67-4.mol

Synonyms:5-iodo-benzofuran;5-Iod-benzofuran;5-Jodbenzonorbornen-2-on;5-iodo-benzobicyclo(2.2.1)hepten-2-one;InChI=1/C11H9IO/c12-9-3-1-2-7-8-4-6(11(7)9)5-10(8)13/h1-3,6,8H,4-5H2;1,4-Methanonaphthalen-2(1H)-one,3,4-dihydro-5-iodo;5-iodobenzonorbornen-2-one;

Chemical Property of 5-Iodobenzofuran

Chemical Property:

• PSA: 13.14000
• LogP: 3.03740

Purity/Quality:

99% ^*data from raw suppliers

5-Iodobenzo[b]furan ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Iodobenzofuran

There total 5 articles about 5-Iodobenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

5-bromobenzofuran (23145-07-5) → 5-iodobenzofuran (60770-67-4)

Guidance literature:

With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; at 110 ℃; for 24h; Sealed tube; Inert atmosphere; Schlenk technique;

DOI:10.1039/d1cc06591b

Reference yield: 71.0%

benzofuran-5-carboxylic acid (90721-27-0) → 5-iodobenzofuran (60770-67-4)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1-iodo-butane; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; chloro-N,N,N',N'-bis(tetramethylene)formamidinium hexafluorophosphate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 120 ℃; for 16h; Sealed tube; Inert atmosphere;

DOI:10.1002/anie.202103269

Reference yield:

1-(2,2-diethoxyethoxy)-4-iodobenzene → 5-iodobenzofuran (60770-67-4)

Guidance literature:

With polyphosphoric acid; In toluene; for 12h; Reflux; Inert atmosphere;

DOI:10.1039/c9cc05563k

upstream raw materials:

p-Iodophenol

benzofuran-5-carboxylic acid

5-bromobenzofuran

Downstream raw materials:

2-(Benzofuran-5-ylthio)-1-(4-methoxybenzyl)-1H-imidazo[4,5-c]pyridin-4-amine

benzo[b]furan-5-carbonitrile

5-benzyl benzofuran

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