9,9-Dimethyl-10-[2-(prop-1-EN-2-YL)phenyl]-9,10-dihydroanthracene

Base Information

• Chemical Name: 9,9-Dimethyl-10-[2-(prop-1-EN-2-YL)phenyl]-9,10-dihydroanthracene
• CAS No.: 60997-90-2
• Molecular Formula: C₂₅H₂₄
• Molecular Weight: 324.466
• DSSTox Substance ID: DTXSID30503832
• Wikidata: Q82357893

Synonyms:60997-90-2;DTXSID30503832;9,9-DIMETHYL-10-[2-(PROP-1-EN-2-YL)PHENYL]-9,10-DIHYDROANTHRACENE

Chemical Property of 9,9-Dimethyl-10-[2-(prop-1-EN-2-YL)phenyl]-9,10-dihydroanthracene

Chemical Property:

• XLogP3: 7.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 324.187800766
• Heavy Atom Count: 25
• Complexity: 460

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C)C1=CC=CC=C1C2C3=CC=CC=C3C(C4=CC=CC=C24)(C)C

Technology Process of 9,9-Dimethyl-10-[2-(prop-1-EN-2-YL)phenyl]-9,10-dihydroanthracene

There total 2 articles about 9,9-Dimethyl-10-[2-(prop-1-EN-2-YL)phenyl]-9,10-dihydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-<9,10-Dihydro-10,10-dimethyl-9-anthryl>-α,α-dimethylbenzolmethanol (60997-89-9) → 9,10-Dihydro-9,9-dimethyl-10-<2-(1-methylethenyl)phenyl>anthracen (60997-90-2)

Guidance literature:

With hydrogenchloride; zinc(II) chloride;

Reference yield:

3',3',10,10-Tetramethyl-spiro (60997-86-6) → 9,10-Dihydro-9,9-dimethyl-10-<2-(1-methylethenyl)phenyl>anthracen (60997-90-2)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) Li, (ii) H₂O

2: ZnCl₂, HCl

With hydrogenchloride; zinc(II) chloride;

Reference yield:

9,10-Dihydro-9,9-dimethyl-10-<2-(1-methylethenyl)phenyl>anthracen (60997-90-2) → 9,10-Dihydro-9,9-dimethyl-10-<2-(1-methylethyl)phenyl>anthracen (76230-16-5)

Guidance literature:

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethyl acetate; for 72h; Yield given;

upstream raw materials:

2-<9,10-Dihydro-10,10-dimethyl-9-anthryl>-α,α-dimethylbenzolmethanol

3',3',10,10-Tetramethyl-spiro

Downstream raw materials:

9,10-Dihydro-9,9-dimethyl-10-<2-(1-methylethyl)phenyl>anthracen

9,10-Dihydro-9-methoxy-10,10-dimethyl-9-<2-(1-methylethyl)phenyl>anthracen

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