Benzeneacetic acid, 4-(1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl)-

Base Information

Chemical Name:Benzeneacetic acid, 4-(1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl)-
CAS No.:108664-26-2
Molecular Formula:C₁₆H₁₃NO₄
Molecular Weight:283.284
Hs Code.:
DSSTox Substance ID:DTXSID30148681
Wikidata:Q83014273

Synonyms:108664-26-2;Benzeneacetic acid, 4-(1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl)-;Benzeneacetic acid, 4-[1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl]-;DTXSID30148681;2-[4-[2-(2-oxo-1-pyridyl)prop-2-enoyl]phenyl]acetic acid

Suppliers and Price of Benzeneacetic acid, 4-(1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzeneacetic acid, 4-(1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl)-

Chemical Property:

Vapor Pressure:3.14E-13mmHg at 25°C
Boiling Point:556.7°Cat760mmHg
Flash Point:290.5°C
Density:1.33g/cm³
XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:283.08445790
Heavy Atom Count:21
Complexity:524

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C(C(=O)C1=CC=C(C=C1)CC(=O)O)N2C=CC=CC2=O

Technology Process of Benzeneacetic acid, 4-(1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl)-

There total 3 articles about Benzeneacetic acid, 4-(1-oxo-2-(2-oxo-1(2H)-pyridinyl)-2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142-08-5,1199357-22-6
2-Pyridone

: 108664-26-2
4-[2-(2-Oxo-2H-pyridin-1-yl)-acryloyl]-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran / 0.5 h / Ambient temperature

2: acetic anhydride / 0.25 h / 40 °C

With acetic anhydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jm00391a037

Reference yield:

: 3609-53-8
methyl 4-acetylbenzoate

: 108664-26-2
4-[2-(2-Oxo-2H-pyridin-1-yl)-acryloyl]-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Br₂ / CHCl₃ / 0.25 h / Ambient temperature

2: NaH / tetrahydrofuran / 0.5 h / Ambient temperature

3: acetic anhydride / 0.25 h / 40 °C

With bromine; acetic anhydride; sodium hydride; In tetrahydrofuran; chloroform;
DOI:10.1021/jm00391a037

Reference yield:

: 56893-25-5
methyl 4-(2-bromoacetyl)benzoate

: 108664-26-2
4-[2-(2-Oxo-2H-pyridin-1-yl)-acryloyl]-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / tetrahydrofuran / 0.5 h / Ambient temperature

2: acetic anhydride / 0.25 h / 40 °C

With acetic anhydride; sodium hydride; In tetrahydrofuran;
DOI:10.1021/jm00391a037