Phosphorane, [(3-nitrophenyl)methylene]triphenyl-

Base Information

Chemical Name:Phosphorane, [(3-nitrophenyl)methylene]triphenyl-
CAS No.:61110-97-2
Molecular Formula:C25H20NO2P
Molecular Weight:397.413
Hs Code.:
DSSTox Substance ID:DTXSID40487891
Wikidata:Q82330200

Synonyms:Phosphorane, [(3-nitrophenyl)methylene]triphenyl-;61110-97-2;SCHEMBL8866275;DTXSID40487891

Suppliers and Price of Phosphorane, [(3-nitrophenyl)methylene]triphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phosphorane, [(3-nitrophenyl)methylene]triphenyl-

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:397.12316588
Heavy Atom Count:29
Complexity:528

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=CC2=CC(=CC=C2)[N+](=O)[O-])(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Phosphorane, [(3-nitrophenyl)methylene]triphenyl-

There total 2 articles about Phosphorane, [(3-nitrophenyl)methylene]triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1530-41-2
(3-nitrobenzyl)(triphenyl)phosphonium bromide

: 61110-97-2
(3-nitrobenzylidene)triphenylphosphorane

Guidance literature:: With sodium amide; In benzene;

Reference yield:

: 603-35-0
triphenylphosphine

: 3958-57-4
1-bromomethyl-3-nitrobenzene

: 61110-97-2
(3-nitrobenzylidene)triphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1.1: Reflux

2.1: potassium tert-butylate / 0.5 h / Schlenk technique

2.2: 1 h / Schlenk technique

With potassium tert-butylate;
DOI:10.1016/j.ejmech.2021.113706