Butanoic acid,2-methyl-,(2R,3S,6S,7R,8R)-3-[[3-(formylamino)-2-hydroxybenzoyl]amino]-8-hexyl-2,6-dimethyl-4,9-dioxo-1,5-dioxonan-7-ylester

Base Information

Chemical Name:Butanoic acid,2-methyl-,(2R,3S,6S,7R,8R)-3-[[3-(formylamino)-2-hydroxybenzoyl]amino]-8-hexyl-2,6-dimethyl-4,9-dioxo-1,5-dioxonan-7-ylester
CAS No.:28068-16-8
Molecular Formula:C28H40 N2 O9
Molecular Weight:548.634
Hs Code.:
Mol file:28068-16-8.mol

Butanoic acid,2-methyl-,(2R,3S,6S,7R,8R)-3-[[3-(formylamino)-2-hydroxybenzoyl]amino]-8-hexyl-2,6-dimethyl-4,9-dioxo-1,5-dioxonan-7-ylester

Synonyms:Butyricacid, 2-methyl-, 8-ester with3-formamido-N-(7-hexyl-8-hydroxy-4,9-dimethyl-2,6-dioxo-1,5-dioxonan-3-yl)salicylamide(8CI); 1,5-Dioxonane, butanoic acid deriv.; Salicylamide,3-formamido-N-(7-hexyl-8-hydroxy-4,9-dimethyl-2,6-dioxo-1,5-dioxonan-3-yl)-,8-(2-methylbutyrate) (8CI); Antimycin A1a

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Chemical Property of Butanoic acid,2-methyl-,(2R,3S,6S,7R,8R)-3-[[3-(formylamino)-2-hydroxybenzoyl]amino]-8-hexyl-2,6-dimethyl-4,9-dioxo-1,5-dioxonan-7-ylester

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Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Butanoic acid,2-methyl-,(2R,3S,6S,7R,8R)-3-[[3-(formylamino)-2-hydroxybenzoyl]amino]-8-hexyl-2,6-dimethyl-4,9-dioxo-1,5-dioxonan-7-ylester

There total 5 articles about Butanoic acid,2-methyl-,(2R,3S,6S,7R,8R)-3-[[3-(formylamino)-2-hydroxybenzoyl]amino]-8-hexyl-2,6-dimethyl-4,9-dioxo-1,5-dioxonan-7-ylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₅H₄₆N₂O₉

: 28068-16-8
antimycin A₁a(S)

Guidance literature:: With palladium on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 2h; under 760.051 Torr;
DOI:10.1002/ejoc.201100034

Reference yield:

: 1309473-53-7
C₂₃H₃₃NO₇

: 28068-16-8
antimycin A₁a(S)

Guidance literature:: Multi-step reaction with 4 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

2: palladium on carbon; hydrogen / tetrahydrofuran / 2 h / 20 °C / 760.05 Torr / Darkness

3: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

4: palladium on carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr

With 4-methyl-morpholine; dmap; palladium on carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100034

Reference yield:

: C₂₈H₄₁NO₈

: 28068-16-8
antimycin A₁a(S)

Guidance literature:: Multi-step reaction with 3 steps

1: palladium on carbon; hydrogen / tetrahydrofuran / 2 h / 20 °C / 760.05 Torr / Darkness

2: 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 24 h / 20 °C

3: palladium on carbon; hydrogen / ethyl acetate / 2 h / 20 °C / 760.05 Torr

With 4-methyl-morpholine; palladium on carbon; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201100034