6-[4-(3,5-dimethylphenyl)-1-buten-3-ynyl]-2,4-dimethylphenanthrene

Base Information

Chemical Name:6-[4-(3,5-dimethylphenyl)-1-buten-3-ynyl]-2,4-dimethylphenanthrene
CAS No.:61172-25-6
Molecular Formula:C₂₈H₂₄
Molecular Weight:360.499
Hs Code.:
Mol file:61172-25-6.mol

Synonyms:

Suppliers and Price of 6-[4-(3,5-dimethylphenyl)-1-buten-3-ynyl]-2,4-dimethylphenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-[4-(3,5-dimethylphenyl)-1-buten-3-ynyl]-2,4-dimethylphenanthrene

Chemical Property:

PSA：0.00000
LogP:7.29150

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-[4-(3,5-dimethylphenyl)-1-buten-3-ynyl]-2,4-dimethylphenanthrene

There total 3 articles about 6-[4-(3,5-dimethylphenyl)-1-buten-3-ynyl]-2,4-dimethylphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52988-44-0
2,4,6-Trimethylphenanthren

: 61172-25-6
6-[(E)-4-(3,5-Dimethyl-phenyl)-but-1-en-3-ynyl]-2,4-dimethyl-phenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: NBS, (PhCO)2O₂ / CCl₄ / Irradiation

2: (i) Ph₃P, xylene, (ii) /BRN= 2356531/, NaOMe, MeOH

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1039/P29760001104

Reference yield:

: 1-(3,3-Diethoxy-prop-1-ynyl)-3,5-dimethyl-benzene

: 61172-25-6
6-[(E)-4-(3,5-Dimethyl-phenyl)-but-1-en-3-ynyl]-2,4-dimethyl-phenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: (acid hydrolysis)

2: (i) Ph₃P, xylene, (ii) /BRN= 2356531/, NaOMe, MeOH

DOI:10.1039/P29760001104