Phosphinous acid, diphenyl-, 1,1-diethylpropyl ester

Base Information

• Chemical Name: Phosphinous acid, diphenyl-, 1,1-diethylpropyl ester
• CAS No.: 612058-37-4
• Molecular Formula: C19H25OP
• Molecular Weight: 300.381

Synonyms:

Chemical Property of Phosphinous acid, diphenyl-, 1,1-diethylpropyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Phosphinous acid, diphenyl-, 1,1-diethylpropyl ester

There total 1 articles about Phosphinous acid, diphenyl-, 1,1-diethylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-ethylpentan-3-ol (597-49-9) + chloro-diphenylphosphine (1079-66-9,74391-44-9) → (1,1-diethylpropoxy)di(phenyl)phosphine (612058-37-4)

Guidance literature:

With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 1h;

DOI:10.1246/cl.2003.300

Reference yield:

3-Phenylpropionic acid (501-52-0) + (1,1-diethylpropoxy)di(phenyl)phosphine (612058-37-4) → 1,1-diethylpropyl 3-phenylpropionate

Guidance literature:

With 2,6-dimethyl-1,4-benzoquinone; In dichloromethane; at 20 ℃; for 15h;

DOI:10.1246/bcsj.76.1645

Reference yield:

benzoic acid (65-85-0,8013-63-6) + (1,1-diethylpropoxy)di(phenyl)phosphine (612058-37-4) → 1,1-diethylpropyl benzoate (23293-74-5)

Guidance literature:

With 2,6-dimethyl-1,4-benzoquinone; In dichloromethane; for 6h; Heating;

DOI:10.1246/cl.2003.300

upstream raw materials:

3-ethylpentan-3-ol

chloro-diphenylphosphine

Downstream raw materials:

1,1-diethylpropyl benzoate

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