4-Chloro-9h-fluoren-2-amine

Base Information

• Chemical Name: 4-Chloro-9h-fluoren-2-amine
• CAS No.: 1785-37-1
• Molecular Formula: C13H10ClN
• Molecular Weight: 215.6782
• NSC Number: 83329
• DSSTox Substance ID: DTXSID50292514
• Wikidata: Q82030848

Synonyms:4-chloro-9h-fluoren-2-amine;1785-37-1;NSC83329;DTXSID50292514;NSC-83329

Chemical Property of 4-Chloro-9h-fluoren-2-amine

Chemical Property:

• Vapor Pressure: 2.76E-07mmHg at 25°C
• Boiling Point: 420.7°Cat760mmHg
• Flash Point: 208.2°C
• Density: 1.326g/cm³
• XLogP3: 3.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 215.0501770
• Heavy Atom Count: 15
• Complexity: 243

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C2=CC=CC=C2C3=C1C=C(C=C3Cl)N

Technology Process of 4-Chloro-9h-fluoren-2-amine

There total 3 articles about 4-Chloro-9h-fluoren-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Chlor-2-nitro-9-oxo-fluoren (1785-34-8) → 2-Amino-4-chlor-fluoren (1785-37-1)

Guidance literature:

With hydrazine hydrate;

DOI:10.1021/jm00328a017

Reference yield:

2-bromobenzoic acid methyl ester (610-94-6) → 2-Amino-4-chlor-fluoren (1785-37-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 210 - 215 °C

2: N₂H₄*H₂O

With hydrazine hydrate;

DOI:10.1021/jm00328a017

Reference yield:

3-chloro-4-iodonitrobenzene (41252-96-4) → 2-Amino-4-chlor-fluoren (1785-37-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 210 - 215 °C

2: N₂H₄*H₂O

With hydrazine hydrate;

DOI:10.1021/jm00328a017

upstream raw materials:

4-Chlor-2-nitro-9-oxo-fluoren

2-bromobenzoic acid methyl ester

3-chloro-4-iodonitrobenzene

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