ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-[1,3]dioxolo[4,5-h]chromene-7-carboxylate

Base Information

Chemical Name:ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-[1,3]dioxolo[4,5-h]chromene-7-carboxylate
CAS No.:116409-03-1
Molecular Formula:C₂₃H₂₄O₈
Molecular Weight:428.439
Hs Code.:
DSSTox Substance ID:DTXSID70922048
Mol file:116409-03-1.mol

Synonyms:116409-03-1;ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-[1,3]dioxolo[4,5-h]chromene-7-carboxylate;8H-1,3-Dioxolo(4,5-h)(1)benzopyran-7-carboxylic acid, 6-methyl-8-(3,4, 5-trimethoxyphenyl)-, ethyl e;Ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-1,3-dioxolo(4,5-h)(1)benzopyran-7-carboxylate;DTXSID70922048;8H-1,3-Dioxolo(4,5-h)(1)benzopyran-7-carboxylic acid, 6-methyl-8-(3,4,5-trimethoxyphenyl)-, ethyl ester;Ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-2H,8H-[1,3]dioxolo[4,5-h][1]benzopyran-7-carboxylate

Suppliers and Price of ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-[1,3]dioxolo[4,5-h]chromene-7-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-[1,3]dioxolo[4,5-h]chromene-7-carboxylate

Chemical Property:

Vapor Pressure:1.35E-11mmHg at 25°C
Boiling Point:536.8°Cat760mmHg
Flash Point:232.3°C
PSA：81.68000
Density:1.267g/cm³
LogP:3.91140
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:7
Exact Mass:428.14711772
Heavy Atom Count:31
Complexity:665

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=C(C2=C(C3=C(C=C2)OCO3)OC1C4=CC(=C(C(=C4)OC)OC)OC)C

Technology Process of ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-[1,3]dioxolo[4,5-h]chromene-7-carboxylate

There total 5 articles about ethyl 6-methyl-8-(3,4,5-trimethoxyphenyl)-8H-[1,3]dioxolo[4,5-h]chromene-7-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 116409-01-9
(7R,8S)-6-Hydroxy-6-methyl-8-(3,4,5-trimethoxy-phenyl)-7,8-dihydro-6H-[1,3]dioxolo[4,5-g]chromene-7-carboxylic acid ethyl ester

: 116409-03-1
6-Methyl-8-(3,4,5-trimethoxy-phenyl)-8H-[1,3]dioxolo[4,5-g]chromene-7-carboxylic acid ethyl ester

Guidance literature:: With hydrogenchloride; acetic acid;
DOI:10.1002/jhet.5570250113

Reference yield:

: 533-31-3
Sesamol

: 116409-03-1
6-Methyl-8-(3,4,5-trimethoxy-phenyl)-8H-[1,3]dioxolo[4,5-g]chromene-7-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / methanol / 0.5 h / Heating

2: 89 percent

3: 63 percent / H₃O⁽¹⁺⁾

4: 95 percent / HOAc, HCl

With hydrogenchloride; oxonium; acetic acid; In methanol;
DOI:10.1002/jhet.5570250113

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 116409-03-1
6-Methyl-8-(3,4,5-trimethoxy-phenyl)-8H-[1,3]dioxolo[4,5-g]chromene-7-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / methanol / 0.5 h / Heating

2: 89 percent

3: 63 percent / H₃O⁽¹⁺⁾

4: 95 percent / HOAc, HCl

With hydrogenchloride; oxonium; acetic acid; In methanol;
DOI:10.1002/jhet.5570250113