2-Cyclopenten-1-ol, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-

Base Information

Chemical Name:2-Cyclopenten-1-ol, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-
CAS No.:61305-33-7
Molecular Formula:C₁₁H₂₂O₂Si
Molecular Weight:214.38
Hs Code.:

Synonyms:(+/-)-(1S,4R)-4-(tert-butyldimethylsilyloxy)cyclopent-2-enol;cis 4-[(1,1-dimethylethyl)dimethylsilyloxy]cyclopent-2-en-1-ol;cis-4-(tert-butyldimethylsilylanyloxy)cyclopent-2-en-1-ol;(+/-)-cis-4-tert-butyldimethylsilyloxy-2-cyclopentenol;cis-4-(tert-butyl-dimethylsilanyloxy)-cyclopent-2-enol;cis-2-cyclopentene-1,4-diol mono-tert-butyldimethylsilyl ether;

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyclopenten-1-ol, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-

Chemical Property:

Boiling Point:245.9±40.0 °C(Predicted)
PSA：29.46000
Density:0.94±0.1 g/cm3(Predicted)
LogP:2.69760

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Cyclopenten-1-ol, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-

There total 1 articles about 2-Cyclopenten-1-ol, 4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1RS,4SR)-4-(tert-butyldimethylsilyloxy)cyclopent-2-enyl picolinate

: 1589-82-8
phenylmagnesium bromide

: C₁₈H₂₈OSi

: 61305-33-7,61692-07-7,61692-08-8,61740-30-5,61740-31-6,81939-24-4,81939-25-5,104069-09-2,120520-91-4
cis-(+/-)-4-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-cyclopenten-1-ol

Guidance literature:: With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 14h;
DOI:10.1021/ol802949c

Reference yield: 97.0%

: 61305-33-7,61692-07-7,61692-08-8,61740-30-5,61740-31-6,81939-24-4,81939-25-5,104069-09-2,120520-91-4
cis-(+/-)-4-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-cyclopenten-1-ol

: 65-85-0,8013-63-6
benzoic acid

: trans-(+/-)-4-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-cyclopenten-1-yl benzoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1021/jo951930h