2-Bromo-1-phenanthren-1-ylethanone

Base Information

Chemical Name:2-Bromo-1-phenanthren-1-ylethanone
CAS No.:26698-40-8
Molecular Formula:C₁₆H₁₁BrO
Molecular Weight:299.167
Hs Code.:
NSC Number:174153
DSSTox Substance ID:DTXSID40306119
Wikidata:Q82053047

Synonyms:26698-40-8;2-bromo-1-phenanthren-1-ylethanone;NSC174153;1-(Bromoacetyl)phenanthrene;DTXSID40306119;WILJFYMOVYNGTC-UHFFFAOYSA-N;2-Bromo-1-(1-phenanthryl)ethanone #;NSC-174153

Suppliers and Price of 2-Bromo-1-phenanthren-1-ylethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Bromo-1-phenanthren-1-ylethanone

Chemical Property:

Vapor Pressure:3.61E-08mmHg at 25°C
Boiling Point:446.6°Cat760mmHg
Flash Point:108.7°C
Density:1.478g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:297.99933
Heavy Atom Count:18
Complexity:314

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC3=C2C=CC=C3C(=O)CBr

Technology Process of 2-Bromo-1-phenanthren-1-ylethanone

There total 5 articles about 2-Bromo-1-phenanthren-1-ylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26698-31-7
2-(Phenanthrene-1-carbonyl)-malonic acid diethyl ester

: 26698-40-8
2-Bromo-1-phenanthren-1-yl-ethanone

Guidance literature:: Multistep reaction; (i) (hydrolysis), (ii) (decarboxylation), (iii) Br₂, AlCl₃, CHCl₃, Et₂O;
DOI:10.1021/jm00296a016

Reference yield:

: 27875-89-4
1-phenanthrenecarboxylic acid

: 26698-40-8
2-Bromo-1-phenanthren-1-yl-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / Heating

3: (i) (hydrolysis), (ii) (decarboxylation), (iii) Br₂, AlCl₃, CHCl₃, Et₂O

With thionyl chloride;
DOI:10.1021/jm00296a016

Reference yield:

: 26698-28-2
Phenanthrene-1-carbonyl chloride

: 26698-40-8
2-Bromo-1-phenanthren-1-yl-ethanone

Guidance literature:: Multi-step reaction with 2 steps

2: (i) (hydrolysis), (ii) (decarboxylation), (iii) Br₂, AlCl₃, CHCl₃, Et₂O

DOI:10.1021/jm00296a016