1,3,4-Thiadiazole-2(3H)-thione, 5-[(2,5-dimethoxyphenyl)amino]-

Base Information

Chemical Name:1,3,4-Thiadiazole-2(3H)-thione, 5-[(2,5-dimethoxyphenyl)amino]-
CAS No.:61335-27-1
Molecular Formula:C10H11N3O2S2
Molecular Weight:269.348
Hs Code.:
DSSTox Substance ID:DTXSID00487837
Wikidata:Q82330110

Synonyms:61335-27-1;1,3,4-Thiadiazole-2(3H)-thione, 5-[(2,5-dimethoxyphenyl)amino]-;DTXSID00487837;AKOS005893264

Suppliers and Price of 1,3,4-Thiadiazole-2(3H)-thione, 5-[(2,5-dimethoxyphenyl)amino]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1,3,4-Thiadiazole-2(3H)-thione, 5-[(2,5-dimethoxyphenyl)amino]-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:269.02926895
Heavy Atom Count:17
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)OC)NC2=NNC(=S)S2

Technology Process of 1,3,4-Thiadiazole-2(3H)-thione, 5-[(2,5-dimethoxyphenyl)amino]-

There total 4 articles about 1,3,4-Thiadiazole-2(3H)-thione, 5-[(2,5-dimethoxyphenyl)amino]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-56-7,102526-87-4
2,5-dimethoxyaniline

: 61335-27-1
5-(2,5-dimethoxy-anilino)-3H-[1,3,4]thiadiazole-2-thione

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / 12 h / Cooling with ice

1.2: 6 h / 25 °C

2.1: hydrazine hydrate / isopropyl alcohol / 2 h / 25 °C

3.1: potassium hydroxide / ethanol / 4 h / Reflux

With hydrazine hydrate; triethylamine; potassium hydroxide; In ethanol; isopropyl alcohol;
DOI:10.1080/10426507.2020.1737062

Reference yield:

: 40532-06-7
2-isothiocyanato-1,4-dimethoxybenzene

: 61335-27-1
5-(2,5-dimethoxy-anilino)-3H-[1,3,4]thiadiazole-2-thione

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / isopropyl alcohol / 2 h / 25 °C

2: potassium hydroxide / ethanol / 4 h / Reflux

With hydrazine hydrate; potassium hydroxide; In ethanol; isopropyl alcohol;
DOI:10.1080/10426507.2020.1737062