Benzaldehyde, 3,4-dibenzyloxy-2-fluoro-

Base Information

Chemical Name:Benzaldehyde, 3,4-dibenzyloxy-2-fluoro-
CAS No.:61338-96-3
Molecular Formula:C21H17FO3
Molecular Weight:336.35600
Hs Code.:
DSSTox Substance ID:DTXSID50340322
Nikkaji Number:J1.553.190H
Wikidata:Q82109898

Synonyms:Benzaldehyde, 3,4-dibenzyloxy-2-fluoro-;61338-96-3;Benzaldehyde, 2-fluoro-3,4-bis(phenylmethoxy)-;SCHEMBL11855056;DTXSID50340322;2-Fluoro-3,4-bis(benzyloxy)benzaldehyde;3,4-Bis(benzyloxy)-2-fluorobenzaldehyde #

Suppliers and Price of Benzaldehyde, 3,4-dibenzyloxy-2-fluoro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzaldehyde, 3,4-dibenzyloxy-2-fluoro-

Chemical Property:

Melting Point:89-90 °C
Boiling Point:487.9±40.0 °C(Predicted)
PSA：35.53000
Density:1.224±0.06 g/cm3(Predicted)
LogP:4.79620
XLogP3:4.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:336.11617256
Heavy Atom Count:25
Complexity:391

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=C(C(=C(C=C2)C=O)F)OCC3=CC=CC=C3

Technology Process of Benzaldehyde, 3,4-dibenzyloxy-2-fluoro-

There total 5 articles about Benzaldehyde, 3,4-dibenzyloxy-2-fluoro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1,2-Bis-benzyloxy-4-dimethoxymethyl-3-fluoro-benzene

: 61338-96-3
3,4-bis(benzyloxy)-2-fluorobenzaldehyde

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 0.5h; Yield given;
DOI:10.1021/jm00348a014

Reference yield:

: 394-64-9
1-fluoro-2,3-dimethoxybenzene

: 61338-96-3
3,4-bis(benzyloxy)-2-fluorobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / TiCl₄ / CH₂Cl₂ / 0 deg C, 0.5 h; RT, 4.5 h

2: 1.) BBr₃

With boron tribromide; titanium tetrachloride; In dichloromethane;
DOI:10.1021/jm00118a019

Reference yield:

: 100-44-7
benzyl chloride

: 61338-96-3
3,4-bis(benzyloxy)-2-fluorobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃, KI / methanol / 24 h / Heating

2: 1 N aq. HCl / ethyl acetate / 0.5 h

With hydrogenchloride; potassium carbonate; potassium iodide; In methanol; ethyl acetate;
DOI:10.1021/jm00348a014