3-(3,4-Dichloroanilino)-1lambda~6~,4,2-dithiazole-1,1(5H)-dione

Base Information

Chemical Name:3-(3,4-Dichloroanilino)-1lambda~6~,4,2-dithiazole-1,1(5H)-dione
CAS No.:61343-68-8
Molecular Formula:C8H6Cl2N2O2S2
Molecular Weight:297.186
Hs Code.:
DSSTox Substance ID:DTXSID10495564
Wikidata:Q82343766

Synonyms:61343-68-8;SCHEMBL13943134;DTXSID10495564;3-(3,4-Dichloroanilino)-1lambda~6~,4,2-dithiazole-1,1(5H)-dione

Suppliers and Price of 3-(3,4-Dichloroanilino)-1lambda~6~,4,2-dithiazole-1,1(5H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-(3,4-Dichloroanilino)-1lambda~6~,4,2-dithiazole-1,1(5H)-dione

Chemical Property:

Boiling Point:437.6±55.0 °C(Predicted)
PSA：92.21000
Density:1.77±0.1 g/cm3(Predicted)
LogP:4.01420
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:295.9247752
Heavy Atom Count:16
Complexity:393

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1SC(=NS1(=O)=O)NC2=CC(=C(C=C2)Cl)Cl

Technology Process of 3-(3,4-Dichloroanilino)-1lambda~6~,4,2-dithiazole-1,1(5H)-dione

There total 2 articles about 3-(3,4-Dichloroanilino)-1lambda~6~,4,2-dithiazole-1,1(5H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.2%

: 21335-43-3
chloromethanesulfonamide

: 3,4-dichlorophenyl isothiocyanate

: 61343-68-8
(3,4-dichloro-phenyl)-(1,1-dioxo-1,5-dihydro-1λ⁶-[1,4,2]dithiazol-3-yl)-amine

Guidance literature:: chloromethanesulfonamide; 3,4-dichlorophenyl isothiocyanate; With sodium hydroxide; In acetone; at 20 - 50 ℃;

With hydrogenchloride; In water; acetone;

Reference yield:

: 21335-43-3
chloromethanesulfonamide

: 6590-94-9
3,4-dichlorophenyl isothiocyanate

: 61343-68-8
(3,4-dichloro-phenyl)-(1,1-dioxo-1,5-dihydro-1λ⁶-[1,4,2]dithiazol-3-yl)-amine

Guidance literature:: With sodium hydroxide; In acetone;

Reference yield: 24.0%

: 61343-68-8
(3,4-dichloro-phenyl)-(1,1-dioxo-1,5-dihydro-1λ⁶-[1,4,2]dithiazol-3-yl)-amine

: 402-23-3
1-bromomethyl-3-trifluoromethylbenzene

: 1041671-40-2
[5-(3-trifluoromethylbenzyl)-1,1-dioxo-1λ6-[1,4,2]dithiazolidin-3-ylidene]-(3,4-dichloro)phenyl-2-amine

Guidance literature:: (3,4-dichloro-phenyl)-(1,1-dioxo-1,5-dihydro-1λ⁶-[1,4,2]dithiazol-3-yl)-amine; With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1h;

1-bromomethyl-3-trifluoromethylbenzene; In tetrahydrofuran; at -78 ℃; for 5h;

With hydrogenchloride; water; In tetrahydrofuran;