Benzo[b]selenophene, 3-chloro-2-phenyl-

Base Information

Chemical Name:Benzo[b]selenophene, 3-chloro-2-phenyl-
CAS No.:61350-51-4
Molecular Formula:C14H9ClSe
Molecular Weight:291.638
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzo[b]selenophene, 3-chloro-2-phenyl-

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzo[b]selenophene, 3-chloro-2-phenyl-

There total 4 articles about Benzo[b]selenophene, 3-chloro-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1-[o-(benzylseleno)phenyl]-2-phenylethyne

: 61350-51-4
3-chloro-2-phenyl-benzo[b]selenophene

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium chloride; In ethanol; at 20 ℃; for 24h; Green chemistry;
DOI:10.1016/j.tetlet.2017.01.007

Reference yield:

: 583-55-1
1-Bromo-2-iodobenzene

: 61350-51-4
3-chloro-2-phenyl-benzo[b]selenophene

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

2.2: 20 °C

3.1: copper(ll) sulfate pentahydrate; sodium chloride / ethanol / 24 h / 20 °C / Green chemistry

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; copper(ll) sulfate pentahydrate; triethylamine; sodium chloride; In tetrahydrofuran; ethanol; 1.1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tetlet.2017.01.007

Reference yield:

: 536-74-3
phenylacetylene

: 61350-51-4
3-chloro-2-phenyl-benzo[b]selenophene

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine; copper(l) iodide

2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C

2.2: 20 °C

3.1: copper(ll) sulfate pentahydrate; sodium chloride / ethanol / 24 h / 20 °C / Green chemistry

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; copper(ll) sulfate pentahydrate; triethylamine; sodium chloride; In tetrahydrofuran; ethanol; 1.1: |Sonogashira Cross-Coupling;
DOI:10.1016/j.tetlet.2017.01.007