Benzenesulfonyl chloride, 4-(phenylazo)-

Base Information

• Chemical Name: Benzenesulfonyl chloride, 4-(phenylazo)-
• CAS No.: 58359-53-8
• Molecular Formula: C₁₂H₉ClN₂O₂S
• Molecular Weight: 280.735
• Hs Code.: 2927000090
• European Community (EC) Number: 637-324-2
• DSSTox Substance ID: DTXSID1069247
• Nikkaji Number: J207.961E
• Mol file: 58359-53-8.mol

Synonyms:58359-53-8;4-Phenylazobenzenesulfonyl Chloride;Benzenesulfonyl chloride, 4-(phenylazo)-;Azobenzene-4-sulfonyl Chloride;4-phenyldiazenylbenzenesulfonyl chloride;(E)-4-(phenyldiazenyl)benzene-1-sulfonyl chloride;102840-82-4;Benzenesulfonyl chloride, 4-(2-phenyldiazenyl)-;benzenesulfonyl chloride, 4-[2-phenyldiazenyl]-;4-(phenylazo)benzenesulfonyl chloride;SCHEMBL48731;4-Azobenzenesulfonyl chloride;DTXSID1069247;4-phenylazophenylsulfonyl chloride;MFCD00024883;AKOS016016563;A1050;CS-0312307;FT-0640523;4-(Phenyldiazenyl)benzene-1-sulfonyl chloride;T71096

Chemical Property of Benzenesulfonyl chloride, 4-(phenylazo)-

Chemical Property:

• Vapor Pressure: 7.69E-07mmHg at 25°C
• Melting Point: 122 °C
• Refractive Index: 1.622
• Boiling Point: 418.9 °C at 760 mmHg
• Flash Point: 207.2 °C
• PSA: 67.24000
• Density: 1.35 g/cm³
• LogP: 5.11030
• Storage Temp.: Refrigerator
• Solubility.: soluble in Benzene
• XLogP3: 4.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 280.0073264
• Heavy Atom Count: 18
• Complexity: 377

Purity/Quality:

98%,99%, ^*data from raw suppliers

Azobenzene-4-sulfonyl Chloride >98.0%(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N=NC2=CC=C(C=C2)S(=O)(=O)Cl

Technology Process of Benzenesulfonyl chloride, 4-(phenylazo)-

There total 3 articles about Benzenesulfonyl chloride, 4-(phenylazo)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-(phenylazo)benzenesulfonyl chloride (102840-82-4,58359-53-8)

Guidance literature:

With chlorosulphuric acid; at 125 ℃;

DOI:10.1021/jo01179a007

Reference yield:

Azobenzene (1227476-15-4) → 4-(phenylazo)benzenesulfonyl chloride (102840-82-4,58359-53-8)

Guidance literature:

With chlorosulphuric acid; at 125 ℃;

DOI:10.1021/jo01179a007

Reference yield:

→ 4-(phenylazo)benzenesulfonyl chloride (102840-82-4,58359-53-8)

Guidance literature:

With phosphorus pentachloride;

upstream raw materials:

Azobenzene

Downstream raw materials:

1-(4-phenylazo-benzenesulfonyl)-piperidine

4-(4-phenylazo-benzenesulfonyl)-morpholine

4-phenylazo-benzenesulfonic acid ethyl ester

4-phenylazo-benzenesulfonic acid-(4-nitro-anilide)