3-(3,4-Dimethoxybenzoyl)-1,2,2-trimethylcyclopentane-1-carboxylic acid

Base Information

Chemical Name:3-(3,4-Dimethoxybenzoyl)-1,2,2-trimethylcyclopentane-1-carboxylic acid
CAS No.:61490-73-1
Molecular Formula:C18H24O5
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID20497413

Synonyms:61490-73-1;3-(3,4-Dimethoxybenzoyl)-1,2,2-trimethylcyclopentane-1-carboxylic acid;SCHEMBL11586677;DTXSID20497413

Suppliers and Price of 3-(3,4-Dimethoxybenzoyl)-1,2,2-trimethylcyclopentane-1-carboxylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3,4-Dimethoxybenzoyl)-1,2,2-trimethylcyclopentane-1-carboxylic acid

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:320.16237386
Heavy Atom Count:23
Complexity:472

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(CCC1(C)C(=O)O)C(=O)C2=CC(=C(C=C2)OC)OC)C

Technology Process of 3-(3,4-Dimethoxybenzoyl)-1,2,2-trimethylcyclopentane-1-carboxylic acid

There total 1 articles about 3-(3,4-Dimethoxybenzoyl)-1,2,2-trimethylcyclopentane-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61490-73-1
3-(3',4'-dimethoxy-benzoyl)-1,2,2-trimethyl-cyclopentane-carboxylic acid

Guidance literature:: Camphersaeureanhydrid, Veratrol, AlCl3;

Reference yield:

: 57078-09-8,61490-73-1,122169-95-3
(1R,3S)-3-(3,4-Dimethoxy-benzoyl)-1,2,2-trimethyl-cyclopentanecarboxylic acid

: 122082-38-6
(1R,3S)-3-{(3,4-Dimethoxy-phenyl)-[(E)-hydroxyimino]-methyl}-1,2,2-trimethyl-cyclopentanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: 71 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

With pyridine; hydroxylamine hydrochloride; In diethyl ether; ethanol;
DOI:10.1016/0223-5234(88)90091-8

Reference yield:

: 57078-09-8,61490-73-1,122169-95-3
(1R,3S)-3-(3,4-Dimethoxy-benzoyl)-1,2,2-trimethyl-cyclopentanecarboxylic acid

: 122082-49-9
(1R,6S)-5-(3,4-Dimethoxy-phenyl)-1,9,9-trimethyl-3-oxa-4-aza-bicyclo[4.2.1]nonane; hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: 71 percent / NH₂OH*HCl, pyridine / ethanol / 4 h / Heating

3: 1.) LiAlH₄; 2.) HCl gas / 1.) ether, reflux, 24 h; 2.) ether

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; hydroxylamine hydrochloride; In diethyl ether; ethanol;
DOI:10.1016/0223-5234(88)90091-8