Technology Process of Benzoic acid, 4-(4-chloro-4-oxobutyl)-, methyl ester
There total 4 articles about Benzoic acid, 4-(4-chloro-4-oxobutyl)-, methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / diethylamine; triphenylphosphine; copper(I) iodide / palladium chloride / 20 °C
2: 100 percent / H2 / Pd/C / methanol / 12 h / 2327.17 - 2585.74 Torr
3: 63 percent / aq. CrO3; sulfuric acid / acetone / 0 - 20 °C
4: oxalyl chloride / CH2Cl2 / 1 h / Heating
With
chromium(VI) oxide; copper(l) iodide; oxalyl dichloride; sulfuric acid; hydrogen; diethylamine; triphenylphosphine;
palladium on activated charcoal; palladium dichloride;
In
methanol; dichloromethane; acetone;
DOI:10.1021/jm040123k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / H2 / Pd/C / methanol / 12 h / 2327.17 - 2585.74 Torr
2: 63 percent / aq. CrO3; sulfuric acid / acetone / 0 - 20 °C
3: oxalyl chloride / CH2Cl2 / 1 h / Heating
With
chromium(VI) oxide; oxalyl dichloride; sulfuric acid; hydrogen;
palladium on activated charcoal;
In
methanol; dichloromethane; acetone;
DOI:10.1021/jm040123k
- Guidance literature:
-
With
oxalyl dichloride;
In
dichloromethane;
for 1h;
Heating;
DOI:10.1021/jm040123k
