3-(4-ACETOXYPHENYL)-1-PROPENE

Base Information

• Chemical Name: 3-(4-ACETOXYPHENYL)-1-PROPENE
• CAS No.: 61499-22-7
• Molecular Formula: C11H12O2
• Molecular Weight: 176.215
• Hs Code.: 2915390090
• Mol file: 61499-22-7.mol

Synonyms:3-(4-ACETOXYPHENYL)-1-PROPENE;Phenol,4-(2-propenyl)-,acetate;chavicol acetate;4-allylphenyl acetate;Acetic acid 4-allyl-phenyl ester;

Chemical Property of 3-(4-ACETOXYPHENYL)-1-PROPENE

Chemical Property:

• Vapor Pressure: 0.02mmHg at 25°C
• Boiling Point: 251.9oC at 760 mmHg
• Flash Point: 95.8oC
• PSA: 26.30000
• Density: 1.027g/cm3
• LogP: 2.34040

Purity/Quality:

99% ^*data from raw suppliers

3-(4-Acetoxyphenyl)-1-propene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(4-ACETOXYPHENYL)-1-PROPENE

There total 5 articles about 3-(4-ACETOXYPHENYL)-1-PROPENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-(prop-2-enyl)phenol (501-92-8) + acetic anhydride (108-24-7) → phenol, 4-(2-propenyl)-, acetate (61499-22-7)

Guidance literature:

With pyridine; at 20 ℃; for 16h;

Reference yield: 61.0%

Estragole (140-67-0) + acetic anhydride (108-24-7) → phenol, 4-(2-propenyl)-, acetate (61499-22-7)

Guidance literature:

FeCl₃-Montmorillonite K-10; at 70 ℃; for 36h;

Reference yield:

4-bromophenyl acetate (1927-95-3) + 2-Allyl-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (72824-04-5) → phenol, 4-(2-propenyl)-, acetate (61499-22-7)

Guidance literature:

With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium carbonate; In 1,4-dioxane; water; Inert atmosphere; Reflux;

upstream raw materials:

Estragole

acetic anhydride

4-(prop-2-enyl)phenol

4-bromo-phenol

Downstream raw materials:

4-(2-fluoro-3-iodopropyl)phenyl acetate

4-(2-fluoroprop-2-enyl)phenyl acetate

4-(2,3-epoxy-2-fluoropropyl)phenyl acetate

4‐((E)-2-formylvinyl)phenyl acetate

Refernces

• 1、 -. "NITRIC OXIDE DONOR NEPRILYSIN INHIBITORS". . . Retrieved 2014/01/07.
• 2、 Boschi, Donatella,Tron, Gian Cesare,Lazzarato, Loretta,Chegaev, Konstantin,Cena, Clara,Di Stilo, Antonella,Giorgis, Marta,Bertinaria, Massimo,Fruttero, Roberta,Gasco, Alberto. "NO-donor phenols: A new class of products endowed with antioxidant and vasodilator properties". . p. 2886 - 2897. Retrieved 2007/10/03.