1-Oxaspiro[2.7]decan-4-one, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-10-(4-hydroxy-1-methylenebutyl)- 8-[(4-methoxyphenyl)methoxy]-7,7-dimethyl-5,9-bis(phenylmethoxy)-, (5R,6R,8R,9S,10S)-

Base Information

Chemical Name:1-Oxaspiro[2.7]decan-4-one, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-10-(4-hydroxy-1-methylenebutyl)- 8-[(4-methoxyphenyl)methoxy]-7,7-dimethyl-5,9-bis(phenylmethoxy)-, (5R,6R,8R,9S,10S)-
CAS No.:615585-03-0
Molecular Formula:C44H60O8Si
Molecular Weight:745.041
Hs Code.:

1-Oxaspiro[2.7]decan-4-one,
6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-10-(4-hydroxy-1-methylenebutyl)-
8-[(4-methoxyphenyl)methoxy]-7,7-dimethyl-5,9-bis(phenylmethoxy)-,
(5R,6R,8R,9S,10S)-

Synonyms:

Suppliers and Price of 1-Oxaspiro[2.7]decan-4-one, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-10-(4-hydroxy-1-methylenebutyl)- 8-[(4-methoxyphenyl)methoxy]-7,7-dimethyl-5,9-bis(phenylmethoxy)-, (5R,6R,8R,9S,10S)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Oxaspiro[2.7]decan-4-one, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-10-(4-hydroxy-1-methylenebutyl)- 8-[(4-methoxyphenyl)methoxy]-7,7-dimethyl-5,9-bis(phenylmethoxy)-, (5R,6R,8R,9S,10S)-

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Oxaspiro[2.7]decan-4-one, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-10-(4-hydroxy-1-methylenebutyl)- 8-[(4-methoxyphenyl)methoxy]-7,7-dimethyl-5,9-bis(phenylmethoxy)-, (5R,6R,8R,9S,10S)-

There total 1 articles about 1-Oxaspiro[2.7]decan-4-one, 6-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-10-(4-hydroxy-1-methylenebutyl)- 8-[(4-methoxyphenyl)methoxy]-7,7-dimethyl-5,9-bis(phenylmethoxy)-, (5R,6R,8R,9S,10S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 677751-21-2
(2R,3R,5R,6S,7R)-2,6-bis(benzyloxy)-3-(t-butyldimethylsilyloxy)-7-(4-hydroxy-1-methylenebutyl)-5-(4-methoxybenzyloxy)-4,4-dimethyl-8-methylenecyclooctanone

: 615585-03-0
(5R,6R,8R,9S,10S)-5,9-bis(benzyloxy)-6-(t-butyldimethylsilyloxy)-10-(4-hydroxy-1-methylenebutyl)-8-(4-methoxybenzyloxy)-7,7-dimethyl-1-oxaspiro[2.7]decan-4-one

Guidance literature:: With sodium hydroxide; dihydrogen peroxide; In methanol; at 0 ℃;
DOI:10.1246/cl.2004.124

Reference yield: 95.0%

: 615585-03-0
(5R,6R,8R,9S,10S)-5,9-bis(benzyloxy)-6-(t-butyldimethylsilyloxy)-10-(4-hydroxy-1-methylenebutyl)-8-(4-methoxybenzyloxy)-7,7-dimethyl-1-oxaspiro[2.7]decan-4-one

: (5S,6R,8R,9S,10S)-6-(tert-butyldimethylsiloxy)-5,9-dibenzyloxy-7,7-dimethyl-10-(4-formylbut-1-en-2-yl)-8-(4-methoxybenzyloxy)-1-oxa-4-oxospiro[2.7]decane

Guidance literature:: With N-chloro-succinimide; 4 A molecular sieve; potassium carbonate; N-(phenylthio)-N-(tert-butyl)amine; In dichloromethane;
DOI:10.1246/cl.2004.124

Reference yield:

: 615585-03-0
(5R,6R,8R,9S,10S)-5,9-bis(benzyloxy)-6-(t-butyldimethylsilyloxy)-10-(4-hydroxy-1-methylenebutyl)-8-(4-methoxybenzyloxy)-7,7-dimethyl-1-oxaspiro[2.7]decan-4-one

: 4-[(4S,5S,6R,8R,9R)-5,9-bis(benzyloxy)-8-(t-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-7,7-dimethyl-10-oxo-1-oxaspiro[2.7]dec-4-yl]pent-4-enal

: 4-[(4S,5S,6R,8R,9R)-5,9-bis(benzyloxy)-8-(t-butyldimethylsilyloxy)-6-(4-methoxybenzyloxy)-7,7-dimethyl-10-oxo-1-oxaspiro[2.7]dec-4-yl]pent-4-enal

Guidance literature:: With N-chloro-succinimide; N-(phenylthio)-N-(tert-butyl)amine; potassium carbonate; 4 A molecular sieve; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1246/bcsj.78.677