1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-4-(2-methoxy-2-oxoethyl)-5-[[4-(2-meth oxy-2-oxoethyl)-3-(3-methoxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]- 1H-pyrrol-2-yl]methyl]-, methyl ester

Base Information

Chemical Name:1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-4-(2-methoxy-2-oxoethyl)-5-[[4-(2-meth oxy-2-oxoethyl)-3-(3-methoxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]- 1H-pyrrol-2-yl]methyl]-, methyl ester
CAS No.:61637-68-1
Molecular Formula:C36H44N2O12
Molecular Weight:696.752
Hs Code.:

1H-Pyrrole-3-propanoic acid,
2-[(1,1-dimethylethoxy)carbonyl]-4-(2-methoxy-2-oxoethyl)-5-[[4-(2-meth
oxy-2-oxoethyl)-3-(3-methoxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]-
1H-pyrrol-2-yl]methyl]-, methyl ester

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Chemical Property of 1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-4-(2-methoxy-2-oxoethyl)-5-[[4-(2-meth oxy-2-oxoethyl)-3-(3-methoxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]- 1H-pyrrol-2-yl]methyl]-, methyl ester

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MSDS Files:: SDS file from LookChem

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Technology Process of 1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-4-(2-methoxy-2-oxoethyl)-5-[[4-(2-meth oxy-2-oxoethyl)-3-(3-methoxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]- 1H-pyrrol-2-yl]methyl]-, methyl ester

There total 1 articles about 1H-Pyrrole-3-propanoic acid, 2-[(1,1-dimethylethoxy)carbonyl]-4-(2-methoxy-2-oxoethyl)-5-[[4-(2-meth oxy-2-oxoethyl)-3-(3-methoxy-3-oxopropyl)-5-[(phenylmethoxy)carbonyl]- 1H-pyrrol-2-yl]methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.5%

: 75975-52-9
3-(2-Methoxycarbonyl-ethyl)-4-methoxycarbonylmethyl-1H-pyrrole-2-carboxylic acid tert-butyl ester

: 51912-05-1
5-acetoxymethyl-4-(2-methoxycarbonyl-ethyl)-3-methoxycarbonylmethyl-pyrrole-2-carboxylic acid benzyl ester

: 61637-68-1
3,4'-bis-(2-methoxycarbonyl-ethyl)-4,3'-bis-methoxycarbonylmethyl-1H,1'H-5,5'-methanediyl-bis-pyrrole-2-carboxylic acid 2'-benzyl ester 2-tert-butyl ester

Guidance literature:: With toluene-4-sulfonic acid; In dichloromethane; for 3h; Ambient temperature;

Reference yield: 87.0%

: 61637-68-1
3,4'-bis-(2-methoxycarbonyl-ethyl)-4,3'-bis-methoxycarbonylmethyl-1H,1'H-5,5'-methanediyl-bis-pyrrole-2-carboxylic acid 2'-benzyl ester 2-tert-butyl ester

: 207974-95-6
1-Benzyloxycarbonyl-9-carboxy-3,8-bis(2-methoxycarbonylethyl)-2,7-bis(methoxycarbonylmethyl)dipyrromethane

Guidance literature:: With tin(IV) chloride; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

: 61637-68-1
3,4'-bis-(2-methoxycarbonyl-ethyl)-4,3'-bis-methoxycarbonylmethyl-1H,1'H-5,5'-methanediyl-bis-pyrrole-2-carboxylic acid 2'-benzyl ester 2-tert-butyl ester

: 1,14-Bis(benzyloxycarbonyl)-3,7,12-tris(2-methoxycarbonylethyl)-2,8,13-tris(methoxycarbonylmethyl)-5,10,15,17-tetrahydrotripyrrin

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / SnCl₄ / CH₂Cl₂ / 2 h / 0 °C

2: 82 percent / p-TsOH / CHCl₃ / 18 h / Ambient temperature

3: 65 percent / pyridine / 16 h / Heating

With pyridine; tin(IV) chloride; toluene-4-sulfonic acid; In dichloromethane; chloroform;