1-Butyl-6-methylcyclohex-1-ene

Base Information

Chemical Name:1-Butyl-6-methylcyclohex-1-ene
CAS No.:61685-33-4
Molecular Formula:C11H20
Molecular Weight:152.28
Hs Code.:
DSSTox Substance ID:DTXSID90518366
Nikkaji Number:J2.629.134H

Synonyms:1-Butyl-6-methylcyclohex-1-ene;61685-33-4;DTXSID90518366

Suppliers and Price of 1-Butyl-6-methylcyclohex-1-ene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Butyl-6-methylcyclohex-1-ene

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:152.156500638
Heavy Atom Count:11
Complexity:133

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCC1=CCCCC1C

Technology Process of 1-Butyl-6-methylcyclohex-1-ene

There total 5 articles about 1-Butyl-6-methylcyclohex-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 693-03-8
n-butyl magnesium bromide

: 583-60-8
2-Methylcyclohexanone

: 61685-33-4
2-n-butyl-3-methylcyclohexene

Guidance literature:: 2-Methylcyclohexanone; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

With chlorophosphoric acid diphenyl ester; In tetrahydrofuran; hexane; at 20 ℃; for 2h;

n-butyl magnesium bromide; With iron(III)-acetylacetonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; at -5 - 20 ℃; for 2h; chemoselective reaction; Further stages;
DOI:10.1055/s-2008-1067194

Reference yield: 61.0%

: 13757-31-8
1-Butyl-2-methyl-cyclohexanol

: 56608-70-9
1-n-butyl-2-methylcyclohexene

: 61685-33-4
2-n-butyl-3-methylcyclohexene

: 114069-71-5
1-[(E)butylidene]-2-methylcyclohexane

Guidance literature:: With phosphoric acid; heating under vacuum;
DOI:10.1021/ja00541a022

Reference yield:

: 583-60-8
2-Methylcyclohexanone

: 61685-33-4
2-n-butyl-3-methylcyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: hexane / 1 h / 25 °C

2: 85percent phosphoric acid / heating under vacuum

With phosphoric acid; In hexane;
DOI:10.1021/ja00541a022