Carbamic acid, [(1S,2E)-1-methyl-1-(1-methylethyl)-3-[(1S,2S,5R)-5-methyl-2-(1-methyl ethyl)cyclohexyl]-2-propenyl]-, 9H-fluoren-9-ylmethyl ester

Base Information

Chemical Name:Carbamic acid, [(1S,2E)-1-methyl-1-(1-methylethyl)-3-[(1S,2S,5R)-5-methyl-2-(1-methyl ethyl)cyclohexyl]-2-propenyl]-, 9H-fluoren-9-ylmethyl ester
CAS No.:616867-23-3
Molecular Formula:C32H43NO2
Molecular Weight:473.699
Hs Code.:

Carbamic acid,
[(1S,2E)-1-methyl-1-(1-methylethyl)-3-[(1S,2S,5R)-5-methyl-2-(1-methyl
ethyl)cyclohexyl]-2-propenyl]-, 9H-fluoren-9-ylmethyl ester

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Chemical Property of Carbamic acid, [(1S,2E)-1-methyl-1-(1-methylethyl)-3-[(1S,2S,5R)-5-methyl-2-(1-methyl ethyl)cyclohexyl]-2-propenyl]-, 9H-fluoren-9-ylmethyl ester

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Technology Process of Carbamic acid, [(1S,2E)-1-methyl-1-(1-methylethyl)-3-[(1S,2S,5R)-5-methyl-2-(1-methyl ethyl)cyclohexyl]-2-propenyl]-, 9H-fluoren-9-ylmethyl ester

There total 3 articles about Carbamic acid, [(1S,2E)-1-methyl-1-(1-methylethyl)-3-[(1S,2S,5R)-5-methyl-2-(1-methyl ethyl)cyclohexyl]-2-propenyl]-, 9H-fluoren-9-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 616867-12-0
(E)-(S)-2-Isopropyl-4-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-2-methyl-but-3-en-1-ol

: 616867-23-3
[(E)-(S)-1-Isopropyl-3-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-1-methyl-allyl]-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Jones reagent / acetone / 6 h / 0 °C

2: diphenylphosphoryl azide; Et₃N / toluene / 1 h / Heating

3: 520 mg / 110 °C

With jones reagent; diphenylphosphoranyl azide; triethylamine; In acetone; toluene; 2: Curtius rearrangement;
DOI:10.1021/ja037078a

Reference yield:

: 616867-22-2
(E)-(S)-2-Isopropyl-4-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-2-methyl-but-3-enoic acid

: 616867-23-3
[(E)-(S)-1-Isopropyl-3-((1S,2S,5R)-2-isopropyl-5-methyl-cyclohexyl)-1-methyl-allyl]-carbamic acid 9H-fluoren-9-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diphenylphosphoryl azide; Et₃N / toluene / 1 h / Heating

2: 520 mg / 110 °C

With diphenylphosphoranyl azide; triethylamine; In toluene; 1: Curtius rearrangement;
DOI:10.1021/ja037078a