1-Azabicyclo[3.1.0]hexane, 6,6-dimethyl-5-phenyl-

Base Information

Chemical Name:1-Azabicyclo[3.1.0]hexane, 6,6-dimethyl-5-phenyl-
CAS No.:61686-98-4
Molecular Formula:C13H17N
Molecular Weight:187.285
Hs Code.:
DSSTox Substance ID:DTXSID30486171

Synonyms:61686-98-4;1-Azabicyclo[3.1.0]hexane, 6,6-dimethyl-5-phenyl-;DTXSID30486171

Suppliers and Price of 1-Azabicyclo[3.1.0]hexane, 6,6-dimethyl-5-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Azabicyclo[3.1.0]hexane, 6,6-dimethyl-5-phenyl-

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:187.136099547
Heavy Atom Count:14
Complexity:240

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C2(N1CCC2)C3=CC=CC=C3)C

Technology Process of 1-Azabicyclo[3.1.0]hexane, 6,6-dimethyl-5-phenyl-

There total 4 articles about 1-Azabicyclo[3.1.0]hexane, 6,6-dimethyl-5-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 61686-97-3
3-(3,3-Dimethyl-2-phenyl-aziridin-2-yl)-propan-1-ol

: 61686-98-4
6,6-Dimethyl-5-phenyl-1-aza-bicyclo[3.1.0]hexane

Guidance literature:: With bromine; triethylamine; triphenylphosphine; In acetonitrile; for 16h; Ambient temperature;
DOI:10.1016/0040-4020(80)80038-X

Reference yield:

: 61686-90-6
dimethyl-3,3 allyl-2 phenyl-2 aziridine

: 61686-98-4
6,6-Dimethyl-5-phenyl-1-aza-bicyclo[3.1.0]hexane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) diborane; 2.)NaOH, H₂O₂ / 1.) THF, r.t.; 2.) alcohol, reflux

2: 64 percent / PPh₃, Br₂, NEt₃ / acetonitrile / 16 h / Ambient temperature

With sodium hydroxide; dihydrogen peroxide; bromine; triethylamine; triphenylphosphine; diborane; In acetonitrile;
DOI:10.1016/0040-4020(80)80038-X

Reference yield:

: 14491-02-2
2,2-dimethyl-3-phenyl-2H-azirine

: 61686-98-4
6,6-Dimethyl-5-phenyl-1-aza-bicyclo[3.1.0]hexane

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / diethyl ether / 2 h / Ambient temperature

2: 1.) diborane; 2.)NaOH, H₂O₂ / 1.) THF, r.t.; 2.) alcohol, reflux

3: 64 percent / PPh₃, Br₂, NEt₃ / acetonitrile / 16 h / Ambient temperature

With sodium hydroxide; dihydrogen peroxide; bromine; triethylamine; triphenylphosphine; diborane; In diethyl ether; acetonitrile;
DOI:10.1016/0040-4020(80)80038-X