1-Ethyl-1-(4-methoxyphenyl)hydrazine

Base Information

• Chemical Name: 1-Ethyl-1-(4-methoxyphenyl)hydrazine
• CAS No.: 61715-71-7
• Molecular Formula: C9H14N2O
• Molecular Weight: 166.223
• DSSTox Substance ID: DTXSID60523447
• Wikidata: Q82389536

Synonyms:1-Ethyl-1-(4-methoxyphenyl)hydrazine;61715-71-7;SCHEMBL2775693;DTXSID60523447

Chemical Property of 1-Ethyl-1-(4-methoxyphenyl)hydrazine

Chemical Property:

• XLogP3: 1.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 166.110613074
• Heavy Atom Count: 12
• Complexity: 122

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(C1=CC=C(C=C1)OC)N

Technology Process of 1-Ethyl-1-(4-methoxyphenyl)hydrazine

There total 2 articles about 1-Ethyl-1-(4-methoxyphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-ethyl-N-(4-methoxyphenyl)nitrous amide (1193343-89-3) → N-ethyl-N-(4-methoxy-phenyl)-hydrazine (61715-71-7)

Guidance literature:

With acetic acid; zinc; at 5 - 10 ℃;

DOI:10.1016/j.bmcl.2009.08.014

Reference yield:

→ N-ethyl-N-(4-methoxy-phenyl)-hydrazine (61715-71-7)

Guidance literature:

N-Nitrosoanilin, Zn, CH3COOH;

Reference yield: 29.0%

3-((2-ethoxy-3,4-dioxocyclobut-1-en-1-yl)amino)-2-hydroxy-N,N-dimethylbenzamide (464913-33-5) + N-ethyl-N-(4-methoxy-phenyl)-hydrazine (61715-71-7) → 3-(2-(2-ethyl-2-(4-methoxyphenyl)hydrazinyl)-3,4-dioxocyclobut-1-enylamino)-2-hydroxy-N,N-dimethylbenzamide (1193343-83-7)

Guidance literature:

In ethanol; at 20 ℃; for 16h;

upstream raw materials:

N-ethyl-N-(4-methoxyphenyl)nitrous amide

Downstream raw materials:

3-(2-(2-ethyl-2-(4-methoxyphenyl)hydrazinyl)-3,4-dioxocyclobut-1-enylamino)-2-hydroxy-N,N-dimethylbenzamide

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