1-Bromo-2-[4-(2-bromophenoxy)butoxy]benzene

Base Information

Chemical Name:1-Bromo-2-[4-(2-bromophenoxy)butoxy]benzene
CAS No.:61739-61-5
Molecular Formula:C16H16Br2O2
Molecular Weight:400.11
Hs Code.:
DSSTox Substance ID:DTXSID30367916
Wikidata:Q82154097

Synonyms:1-bromo-2-[4-(2-bromophenoxy)butoxy]benzene;61739-61-5;Benzene, 1,1'-[1,4-butanediylbis(oxy)]bis[2-bromo-;SCHEMBL2344935;DTXSID30367916

Suppliers and Price of 1-Bromo-2-[4-(2-bromophenoxy)butoxy]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Bromo-2-[4-(2-bromophenoxy)butoxy]benzene

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:399.94966
Heavy Atom Count:20
Complexity:237

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)OCCCCOC2=CC=CC=C2Br)Br

Technology Process of 1-Bromo-2-[4-(2-bromophenoxy)butoxy]benzene

There total 1 articles about 1-Bromo-2-[4-(2-bromophenoxy)butoxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 110-52-1
1,4-dibromo-butane

: 95-56-7
2-hydroxybromobenzene

: 61739-61-5
1-bromo-2-[4-(2-bromophenoxy)butoxy]benzene

Guidance literature:: 2-hydroxybromobenzene; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

1,4-dibromo-butane; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejic.201900716

Reference yield: 84.0%

: 5419-55-6
Triisopropyl borate

: 61739-61-5
1-bromo-2-[4-(2-bromophenoxy)butoxy]benzene

: 1220624-98-5
(butane-1,4-diylbis(oxy))bis(2,1-phenylene)diboronic acid

Guidance literature:: 1-bromo-2-[4-(2-bromophenoxy)butoxy]benzene; With n-butyllithium; In diethyl ether; hexane; at -78 ℃;

Triisopropyl borate; In diethyl ether; hexane; at -78 - 20 ℃; for 16h;

With water; In diethyl ether; hexane; Acidic conditions;
DOI:10.1002/ejic.201900716

Reference yield: 75.0%

: 22330-25-2,69460-31-7,70492-63-6
trans-dibromobis(diethylphenylphosphine)nickel(II)

: 61739-61-5
1-bromo-2-[4-(2-bromophenoxy)butoxy]benzene

: 61919-77-5
bis(diethylphenylphosphine)[2,2'-(tetramethylenedioxydiphenyl)]nickel(II)

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; benzene; stirring of ligand precursor (in THF) with BuLi (in hexane) for 15 min, addn. of suspn. of Ni-complex (in C6H6), stirring for 20 h; evapn., extn. into hot heptane, volume reduction (crystn.); elem. anal.;
DOI:10.1039/DT9760002053