2-BroMo-M-iodoacetophenone

Base Information

• Chemical Name: 2-BroMo-M-iodoacetophenone
• CAS No.: 61858-38-6
• Molecular Formula: C8H6BrIO
• Molecular Weight: 324.944
• Hs Code.: 2914790090
• Mol file: 61858-38-6.mol

Synonyms:2-Bromo-3'-iodoacetophenone;m-Jod-phenacyl-bromid;2-bromo-1-(3-iodophenyl)ethan-1-one;2-bromo-1-(3-iodo-phenyl)-ethanone;m-Iod-phenacylbromid;2-Brom-1-(3-jod-phenyl)-aethanon;3-iodophenacyl bromide;

Chemical Property of 2-BroMo-M-iodoacetophenone

Chemical Property:

• PSA: 17.07000
• LogP: 2.86880

Purity/Quality:

98%+ ^*data from raw suppliers

3-Iodophenacyl bromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-BroMo-M-iodoacetophenone

There total 7 articles about 2-BroMo-M-iodoacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3-Iodobenzoic acid (618-51-9) → 2-bromo-1-(3-iodophenyl)ethan-1-one (61858-38-6)

Guidance literature:

3-Iodobenzoic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 1h;

diazomethane; In diethyl ether; dichloromethane; at 0 ℃; for 1h;

With hydrogen bromide; In diethyl ether; dichloromethane; Further stages.;

DOI:10.1021/jo800618q

Reference yield: 98.0%

→ 2-bromo-1-(3-iodophenyl)ethan-1-one (61858-38-6)

Guidance literature:

Reference yield: 67.0%

3'-iodoacetophenone (14452-30-3) → 2-bromo-1-(3-iodophenyl)ethan-1-one (61858-38-6)

Guidance literature:

With copper(ll) bromide; In chloroform; ethyl acetate; for 3.5h; Reflux;

DOI:10.1016/j.bmc.2017.05.031

upstream raw materials:

diazomethane

3-Iodobenzoic acid

3'-iodoacetophenone

3-iodobenzoyl chloride

Downstream raw materials:

N-(3-Iodphenacyl)cyclopropylamin

2-amino-5-(3-iodophenyl)imidazole-1-carboxylic acid tert-butyl ester

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