N-methyl-N-phenylhexa-2,4-dienamide

Base Information

Chemical Name:N-methyl-N-phenylhexa-2,4-dienamide
CAS No.:61859-43-6
Molecular Formula:C13H15NO
Molecular Weight:201.268
Hs Code.:
DSSTox Substance ID:DTXSID90295286

Synonyms:N-methyl-N-phenylhexa-2,4-dienamide;61859-43-6;NCIOpen2_006897;DTXSID90295286;AKOS034160944

Suppliers and Price of N-methyl-N-phenylhexa-2,4-dienamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-phenylhexa-2,4-dienamide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:201.115364102
Heavy Atom Count:15
Complexity:249

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC=CC=CC(=O)N(C)C1=CC=CC=C1

Technology Process of N-methyl-N-phenylhexa-2,4-dienamide

There total 5 articles about N-methyl-N-phenylhexa-2,4-dienamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 110-44-1,91751-55-2
sorbic Acid

: 100-61-8
N-methylaniline

: 61859-43-6
(2E,4E)-N-methyl-N-phenyl-2,4-hexadienamide

Guidance literature:: sorbic Acid; With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

N-methylaniline; With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/anie.201808392

Reference yield:

: 14506-08-2
hexa-2t,4t-dienoyl-carbonic acid ethyl ester

: 100-61-8
N-methylaniline

: 61859-43-6
(2E,4E)-N-methyl-N-phenyl-2,4-hexadienamide

Guidance literature:: With toluene;
DOI:10.1021/jo01102a019

Reference yield:

: 142-83-6,4488-48-6
trans,trans-2,4-Hexadienal

: 61859-43-6
(2E,4E)-N-methyl-N-phenyl-2,4-hexadienamide

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) lithium diisopropylamide, 2.) O₂ / 1.) THF, hexane, -78 deg C, 45 min, 2.) a) -78 deg C -> room temperature, b) 2 h

With oxygen; lithium diisopropyl amide;