Cyclohexanone, 2,2-dimethyl-6-(2-oxopropyl)-

Base Information

Chemical Name:Cyclohexanone, 2,2-dimethyl-6-(2-oxopropyl)-
CAS No.:61879-68-3
Molecular Formula:C11H18O2
Molecular Weight:182.263
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexanone, 2,2-dimethyl-6-(2-oxopropyl)-

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Technology Process of Cyclohexanone, 2,2-dimethyl-6-(2-oxopropyl)-

There total 5 articles about Cyclohexanone, 2,2-dimethyl-6-(2-oxopropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 89328-75-6
(+/-)-2,2-dimethyl-6-propenylcyclohexanone

: 61879-68-3
2,2-dimethyl-6-(2-oxopropyl)cyclohexanone

Guidance literature:: With oxygen; copper(II) acetate monohydrate; palladium dichloride; In water; at -78 - 20 ℃;

Reference yield: 14.54%

: 1193-47-1
2,2-dimethyl-cyclohexanone

: 105104-40-3
Okahara's reagent

: 61879-68-3
2,2-dimethyl-6-(2-oxopropyl)cyclohexanone

Guidance literature:: 2,2-dimethyl-cyclohexanone; With sodium hydride; In toluene; at 20 - 40 ℃;

Okahara's reagent; In toluene; at 120 ℃;

With sulfuric acid; In 1,4-dioxane; water; at 60 ℃; for 1h;

Reference yield:

: 583-60-8
2-Methylcyclohexanone

: 61879-68-3
2,2-dimethyl-6-(2-oxopropyl)cyclohexanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium methylate / toluene / 20 °C / Cooling with ice

2.1: potassium carbonate / acetone / Reflux

3.1: potassium tert-butylate / tetrahydrofuran / 0.17 h / 0 °C

3.2: 20 °C / Reflux

3.3: 24 h / Reflux

4.1: potassium tert-butylate / tert-butyl alcohol / 20 °C

4.2: 20 °C

5.1: palladium dichloride; oxygen; copper(II) acetate monohydrate / water / -78 - 20 °C

With potassium tert-butylate; oxygen; sodium methylate; copper(II) acetate monohydrate; potassium carbonate; palladium dichloride; In tetrahydrofuran; water; acetone; toluene; tert-butyl alcohol;