(E)-3-chloro-2-ethylbut-2-enal

Base Information

Chemical Name:(E)-3-chloro-2-ethylbut-2-enal
CAS No.:61958-17-6
Molecular Formula:C₆H₉ClO
Molecular Weight:132.59
Hs Code.:

Synonyms:3-chloro-2-ethyl-2-butenal;2-Chlormethyl-2-aethyl-aethylenoxyd;Aethylepichlorhydrin;2-Aethyl-epichlorhydrin 1,2-Epoxy-2-chlormethyl-butan;2-ethyl-3-chloro-1,2-epoxypropane;2-chloromethyl-2-ethyl-oxirane;3-chloro-2-ethyl-1,2-epoxypropan;

Suppliers and Price of (E)-3-chloro-2-ethylbut-2-enal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of (E)-3-chloro-2-ethylbut-2-enal

Chemical Property:

Boiling Point:178℃
Flash Point:76℃
PSA：17.07000
Density:1.023
LogP:2.10810

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (E)-3-chloro-2-ethylbut-2-enal

There total 1 articles about (E)-3-chloro-2-ethylbut-2-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-87-9
2-Pentanone

: 61958-16-5
(Z)-3-Chlor-2-ethyl-2-butenal

: 61958-17-6
(E)-3-Chlor-2-ethyl-2-butenal

Guidance literature:: Title compound not separated from byproducts;

Reference yield: 39.0%

: 72433-45-5
1-(4-aminophenyl)-2-phenylethan-1-one

: 61958-17-6
(E)-3-Chlor-2-ethyl-2-butenal

: 1-(3-ethyl-2-methyl-quinolin-6-yl)-2-phenyl-ethanone

Guidance literature:: With acetic acid; for 15h; Heating;
DOI:10.1021/jm049499o

Reference yield:

: 61958-17-6
(E)-3-Chlor-2-ethyl-2-butenal

: 2-(3,4-dimethoxy-phenyl)-1-(3-ethyl-2-methyl-quinolin-6-yl)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: AcOH / 8 h / Heating

2.1: n-BuLi / tetrahydrofuran; hexane / -78 °C

2.2: 13 percent / tetrahydrofuran; hexane / -78 - -20 °C

With n-butyllithium; acetic acid; In tetrahydrofuran; hexane;
DOI:10.1021/jm049499o