N-Benzyl-5-nitropyridine-3-sulfonamide

Base Information

Chemical Name:N-Benzyl-5-nitropyridine-3-sulfonamide
CAS No.:62009-15-8
Molecular Formula:C₁₂H₁₁N₃O₄S
Molecular Weight:293.303
Hs Code.:
ChEMBL ID:CHEMBL28068
DSSTox Substance ID:DTXSID90506809
Wikidata:Q82362747

Synonyms:62009-15-8;N-Benzyl-5-nitropyridine-3-sulfonamide;CHEMBL28068;DTXSID90506809

Suppliers and Price of N-Benzyl-5-nitropyridine-3-sulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzyl-5-nitropyridine-3-sulfonamide

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:293.04702701
Heavy Atom Count:20
Complexity:423

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)CNS(=O)(=O)C2=CN=CC(=C2)[N+](=O)[O-]

Technology Process of N-Benzyl-5-nitropyridine-3-sulfonamide

There total 6 articles about N-Benzyl-5-nitropyridine-3-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62009-35-2
5-aminopyridine-3-sulfonic acid

: 62009-15-8
N-benzyl 5-nitro-3-pyridinesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: conc. H₂SO₄, 30percent H₂O₂ / 40 h / Ambient temperature

2: PCl₅, POCl₃ / 6 h / Heating

3: 1 h / Ambient temperature

With phosphorus pentachloride; sulfuric acid; dihydrogen peroxide; trichlorophosphate;
DOI:10.1021/jm00186a017

Reference yield:

: 65001-21-0
5-bromopyridine-3-sulphonyl chloride

: 62009-15-8
N-benzyl 5-nitro-3-pyridinesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: H₂O / 1.5 h / 80 - 90 °C

2: 85.3 percent / CuSO₄*5H₂O, conc. NH₄OH / 20 h / 170 °C

3: conc. H₂SO₄, 30percent H₂O₂ / 40 h / Ambient temperature

4: PCl₅, POCl₃ / 6 h / Heating

5: 1 h / Ambient temperature

With ammonium hydroxide; phosphorus pentachloride; sulfuric acid; water; dihydrogen peroxide; copper(II) sulfate; trichlorophosphate;
DOI:10.1021/jm00186a017

Reference yield:

: 62009-34-1
5-bromopyridine-3-sulfonic acid

: 62009-15-8
N-benzyl 5-nitro-3-pyridinesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85.3 percent / CuSO₄*5H₂O, conc. NH₄OH / 20 h / 170 °C

2: conc. H₂SO₄, 30percent H₂O₂ / 40 h / Ambient temperature

3: PCl₅, POCl₃ / 6 h / Heating

4: 1 h / Ambient temperature

With ammonium hydroxide; phosphorus pentachloride; sulfuric acid; dihydrogen peroxide; copper(II) sulfate; trichlorophosphate;
DOI:10.1021/jm00186a017