2,6-dinitrophenyl acetate

Base Information

• Chemical Name: 2,6-dinitrophenyl acetate
• CAS No.: 1523-09-7
• Molecular Formula: C8H6 N2 O6
• Molecular Weight: 226.145
• Mol file: 1523-09-7.mol

Synonyms:Phenol,2,6-dinitro-, acetate (7CI); Phenol, 2,6-dinitro-, acetate (ester) (8CI,9CI);2,6-Dinitrophenyl acetate; NSC 294823

Chemical Property of 2,6-dinitrophenyl acetate

Chemical Property:

• Vapor Pressure: 2.53E-05mmHg at 25°C
• Boiling Point: 358.5°Cat760mmHg
• Flash Point: 175.1°C
• Density: 1.5g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-dinitrophenyl acetate

There total 2 articles about 2,6-dinitrophenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2,6-dinitrophenol (573-56-8) + acetic anhydride (108-24-7) → 2,6-dinitrophenyl acetate (1523-09-7)

Guidance literature:

With 2,3,4,5,7,8,9,10-octahydropyrimido[1,2-a]azepin-1-ium acetate; In neat (no solvent); at 50 ℃; for 1h; Green chemistry;

DOI:10.1007/s00706-012-0820-7

Reference yield:

→ 2,6-dinitrophenyl acetate (1523-09-7)

Guidance literature:

2,6-Dinitro-phenol, Acetanhydrid, konz. H2SO4;

Reference yield:

2,6-dinitrophenyl acetate (1523-09-7) + 4-cyanophenolate (14609-76-8) → 4-cyanophenyl acetate (13031-41-9) + 2,6-dinitrophenoxide ion (20650-73-1)

Guidance literature:

In water; at 25 ℃; Rate constant; ionic strength - 0.1 M KCl;

DOI:10.1021/ja00189a045

upstream raw materials:

2,6-dinitrophenol

acetic anhydride

Downstream raw materials:

4-cyanophenyl acetate

2,6-dinitrophenoxide ion

4-formylphenyl acetate

Refernces