1,3-Dimethyl-1H-pyrazol-5-yl 2,4-dichlorobenzoate

Base Information

Chemical Name:1,3-Dimethyl-1H-pyrazol-5-yl 2,4-dichlorobenzoate
CAS No.:62031-00-9
Molecular Formula:C12H10Cl2N2O2
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID80533689
Nikkaji Number:J26.563B
Wikidata:Q63399016

Synonyms:62031-00-9;1,3-Dimethyl-1H-pyrazol-5-yl 2,4-dichlorobenzoate;SCHEMBL11313311;DTXSID80533689;Q63399016;1,3-DIMETHYL-5-PYLAZOLYL-2,4-DICHLOROBENZOATE

Suppliers and Price of 1,3-Dimethyl-1H-pyrazol-5-yl 2,4-dichlorobenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-Dimethyl-1H-pyrazol-5-yl 2,4-dichlorobenzoate

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:284.0119330
Heavy Atom Count:18
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=NN(C(=C1)OC(=O)C2=C(C=C(C=C2)Cl)Cl)C

Technology Process of 1,3-Dimethyl-1H-pyrazol-5-yl 2,4-dichlorobenzoate

There total 2 articles about 1,3-Dimethyl-1H-pyrazol-5-yl 2,4-dichlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2749-59-9
1,3-dimethyl-5-pyrazolone

: 89-75-8
2,4-dichlorobenzoyl chloride

: 62031-00-9
5-(2,4-dichloro-benzoyloxy)-1,3-dimethyl-1H-pyrazole

Guidance literature:: With triethylamine; In dichloromethane; Reflux;
DOI:10.1080/10426507.2013.829832

Reference yield:

: 62031-00-9
5-(2,4-dichloro-benzoyloxy)-1,3-dimethyl-1H-pyrazole

Guidance literature:: 2,4-Dichlor-benzoylchlorid, 1,3-Dimethyl-pyrazolon/Na2CO3(s. CH 601251 <1978> 8);

Reference yield:

: 62031-00-9
5-(2,4-dichloro-benzoyloxy)-1,3-dimethyl-1H-pyrazole

: 1581307-16-5
(2,4-dichlorophenyl)(1,3-dimethyl-5-(phenylthio)-1H-pyrazol-4-yl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / 1,4-dioxane / Reflux

2.1: trichlorophosphate / 6 h / Reflux

3.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

3.2: 24 h / 20 °C

With sodium hydride; potassium carbonate; trichlorophosphate; In tetrahydrofuran; 1,4-dioxane; 1.1: |Fries Phenol Ester Rearrangement;
DOI:10.1080/10426507.2013.829832