Technology Process of 2-Amino-5-cyclopentylpentanoic acid
There total 4 articles about 2-Amino-5-cyclopentylpentanoic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane; water;
at 80 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C / Cooling with ice
2.1: sodium t-butanolate / tetrahydrofuran / 1 h / Cooling with ice
2.2: 20 °C
3.1: palladium 10% on activated carbon; hydrogen / methanol / 17 h / 20 °C
4.1: hydrogenchloride / 1,4-dioxane; water / 5 h / 80 °C
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium t-butanolate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium t-butanolate / tetrahydrofuran / 1 h / Cooling with ice
1.2: 20 °C
2.1: palladium 10% on activated carbon; hydrogen / methanol / 17 h / 20 °C
3.1: hydrogenchloride / 1,4-dioxane; water / 5 h / 80 °C
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; sodium t-butanolate;
In
tetrahydrofuran; 1,4-dioxane; methanol; water;
