1-Cyclohexene-1-carboxylic acid, 5-(1,1-dimethylethyl)-, ethyl ester

Base Information

Chemical Name:1-Cyclohexene-1-carboxylic acid, 5-(1,1-dimethylethyl)-, ethyl ester
CAS No.:62222-98-4
Molecular Formula:C13H22O2
Molecular Weight:210.31300
Hs Code.:

Synonyms:5-tert-Butylcyclohex-1-enecarboxylic acid ethyl ester;1-Cyclohexene-1-carboxylic acid,5-(1,1-dimethylethyl)-,ethyl ester;4-tert.-Butylcyclohex-1-encarbonsaeureethylester;

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Chemical Property of 1-Cyclohexene-1-carboxylic acid, 5-(1,1-dimethylethyl)-, ethyl ester

Chemical Property:

PSA：26.30000
LogP:3.32210

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Cyclohexene-1-carboxylic acid, 5-(1,1-dimethylethyl)-, ethyl ester

There total 3 articles about 1-Cyclohexene-1-carboxylic acid, 5-(1,1-dimethylethyl)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: Ethyl 1-[(diethoxyphosphoryl)sulfanyl]-5-tert-butyl-2-oxocyclohexanecarboxylate

: 62222-98-4
5-tert-Butylcyclohex-1-enecarboxylic acid ethyl ester

: Ethyl 2-[(diethoxyphosphoryl)oxy]-5-tert-butyl-1-sulfanylcyclohexanecarboxylate

Guidance literature:: With sodium tetrahydroborate; In methanol; dichloromethane; at -78 ℃; for 3h;
DOI:10.1039/b207700k

Reference yield:

: 40571-96-8,40571-97-9,13049-54-2
ethyl 5-(tert-butyl)-2-oxocyclohexanecarboxylate

: 62222-98-4
5-tert-Butylcyclohex-1-enecarboxylic acid ethyl ester

Guidance literature:: Multistep reaction; (i) H₂, Raney-Ni, EtOH, (ii) POCl₃, Py;

Reference yield:

: 98-53-3
4-tercbutyl-cyclohexanone

: 62222-98-4
5-tert-Butylcyclohex-1-enecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaOEt / ethanol

2: (i) H₂, Raney-Ni, EtOH, (ii) POCl₃, Py

With sodium ethanolate; In ethanol;