Technology Process of Rhenium fluoride oxide(ReF5O), (OC-6-21)- (9CI)
There total 1 articles about Rhenium fluoride oxide(ReF5O), (OC-6-21)- (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
neat (no solvent);
anhydrous conditions, prefluorinated Ni apparatus; 525 K; removal of volatiles (room temp.), vac. sublimation;
DOI:10.1039/DT9910003127
- Guidance literature:
-
With
H2;
In
neat (no solvent);
anhydrous atmosphere; activation of Re by static hydrogenation (573 K), then heating with ReOF5 (stainless-steel autoclave, 473 K, 16 h); cooling to room temp., removal of volatiles (vac.);
DOI:10.1039/DT9910003127