3-(3,4-Dichlorophenyl)prop-2-enal

Base Information

Chemical Name:3-(3,4-Dichlorophenyl)prop-2-enal
CAS No.:62374-02-1
Molecular Formula:C9H6Cl2O
Molecular Weight:201.052
Hs Code.:
European Community (EC) Number:879-459-1
Nikkaji Number:J2.875.573B

Synonyms:3-(3,4-Dichlorophenyl)prop-2-enal;62374-02-1;(E)-3-(3,4-dichlorophenyl)prop-2-enal;(2E)-3-(3,4-DICHLOROPHENYL)PROP-2-ENAL;3,4-dichloro-cinnamaldehyde;KRIZSOUMJXQNGU-OWOJBTEDSA-N;(E)-3-(3,4-Dichlorophenyl)acrylaldehyde;(trans)-3-(3,4-Dichlorophenyl)-2-propenal;EN300-192925;G54399;EN300-6486198;Z1269224361

Suppliers and Price of 3-(3,4-Dichlorophenyl)prop-2-enal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-(3,4-Dichlorophenyl)prop-2-enal

Chemical Property:

Melting Point:92-94 °C
Boiling Point:333.0±32.0 °C(Predicted)
PSA：17.07000
Density:1.325±0.06 g/cm3(Predicted)
LogP:3.20550
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:199.9795702
Heavy Atom Count:12
Complexity:179

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1C=CC=O)Cl)Cl
Isomeric SMILES:C1=CC(=C(C=C1/C=C/C=O)Cl)Cl

Technology Process of 3-(3,4-Dichlorophenyl)prop-2-enal

There total 12 articles about 3-(3,4-Dichlorophenyl)prop-2-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 867-13-0
diethoxyphosphoryl-acetic acid ethyl ester

: 6287-38-3
3,4-dichlorobenzaldehyde

: 62374-02-1
(E)-3,4-dichlorocinnamaldehyde

Guidance literature:: 3,4-dichlorobenzaldehyde; With chloromethyl methyl ether; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 20 ℃; for 0.5h;

diethoxyphosphoryl-acetic acid ethyl ester; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 0.25h; Further stages; Inert atmosphere;
DOI:10.1021/acs.orglett.1c02408

Reference yield: 77.0%

: 29805-14-9
1-(3',4'-dichlorophenyl)prop-2-yn-1-ol

: 62374-02-1
(E)-3,4-dichlorocinnamaldehyde

Guidance literature:: With water; bis(triphenyl)oxodiphosphonium trifluoromethanesulfonate salt; triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.2174/1570178615666180329154246

Reference yield: 73.0%

: 1-(3,4-dichlorophenyl)propene

: 62374-02-1,33802-85-6
3-(3,4-dichlorophenyl)acrylaldehyde

Guidance literature:: With tert.-butylhydroperoxide; Ru(2,4,13,15-tetraphenyl-1,5,12,16-tetraaza-tricyclo[14.2.2.06,11]eicosa-4,6⁽¹¹⁾,7,9,12-pentaene)Cl₂; In acetonitrile; at 20 ℃; for 3h; Reagent/catalyst; Irradiation;
DOI:10.1016/j.poly.2019.05.065