1,1'-(2-Bromo-2-phenylethene-1,1-diyl)bis(2-methoxybenzene)

Base Information

Chemical Name:1,1'-(2-Bromo-2-phenylethene-1,1-diyl)bis(2-methoxybenzene)
CAS No.:62378-32-9
Molecular Formula:C22H19BrO2
Molecular Weight:395.296
Hs Code.:
DSSTox Substance ID:DTXSID40511665
Nikkaji Number:J1.087.896I

Synonyms:62378-32-9;DTXSID40511665;1,1'-(2-Bromo-2-phenylethene-1,1-diyl)bis(2-methoxybenzene)

Suppliers and Price of 1,1'-(2-Bromo-2-phenylethene-1,1-diyl)bis(2-methoxybenzene)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,1'-(2-Bromo-2-phenylethene-1,1-diyl)bis(2-methoxybenzene)

Chemical Property:

XLogP3:6.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:394.05684
Heavy Atom Count:25
Complexity:415

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1C(=C(C2=CC=CC=C2)Br)C3=CC=CC=C3OC

Technology Process of 1,1'-(2-Bromo-2-phenylethene-1,1-diyl)bis(2-methoxybenzene)

There total 4 articles about 1,1'-(2-Bromo-2-phenylethene-1,1-diyl)bis(2-methoxybenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 62378-39-6
1-methoxy-2-[1-(2-methoxyphenyl)-2-phenylvinyl]benzene

: 62378-32-9
2,2-bis(2-methoxyphenyl)-1-phenylvinyl bromide

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; for 1h; Reflux; Irradiation; Inert atmosphere;
DOI:10.1039/b811362a

Reference yield:

: 578-57-4
2-bromoanisole

: 62378-32-9
2,2-bis(2-methoxyphenyl)-1-phenylvinyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: (i) Mg, Et₂O, (ii) /BRN= 509140/, benzene

2: aq. H₃PO₄

3: NBS, (PhCO)2O₂ / CCl₄ / Irradiation

With N-Bromosuccinimide; phosphoric acid; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1246/bcsj.49.2560

Reference yield:

: 62378-38-5
1,1-bis(2-methoxyphenyl)-2-phenylethanol

: 62378-32-9
2,2-bis(2-methoxyphenyl)-1-phenylvinyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: aq. H₃PO₄

2: NBS, (PhCO)2O₂ / CCl₄ / Irradiation

With N-Bromosuccinimide; phosphoric acid; dibenzoyl peroxide; In tetrachloromethane;
DOI:10.1246/bcsj.49.2560