Ethyl 5-methyl-4-phenylthiophene-2-carboxylate

Base Information

Chemical Name:Ethyl 5-methyl-4-phenylthiophene-2-carboxylate
CAS No.:62404-01-7
Molecular Formula:C14H14O2S
Molecular Weight:246.32500
Hs Code.:
DSSTox Substance ID:DTXSID90488934
Wikidata:Q82331926

Synonyms:Ethyl 5-methyl-4-phenylthiophene-2-carboxylate;62404-01-7;SCHEMBL6018784;DTXSID90488934

Suppliers and Price of Ethyl 5-methyl-4-phenylthiophene-2-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of Ethyl 5-methyl-4-phenylthiophene-2-carboxylate

Chemical Property:

PSA：54.54000
LogP:3.90020
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:246.07145086
Heavy Atom Count:17
Complexity:261

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC(=C(S1)C)C2=CC=CC=C2

Technology Process of Ethyl 5-methyl-4-phenylthiophene-2-carboxylate

There total 2 articles about Ethyl 5-methyl-4-phenylthiophene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31357-83-2,31357-84-3,39831-17-9
3-chloro-2-phenyl-but-2-enal

: 623-51-8
ethyl 2-sulfanylacetate

: 62404-01-7
C₁₄H₁₄O₂S

Guidance literature:: With sodium; In ethanol; at 20 - 70 ℃; for 18h;

Reference yield:

: 103-79-7,136675-26-8
1-phenyl-acetone

: 62404-01-7
C₁₄H₁₄O₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / 0.67 h / 5 - 20 °C

1.2: 4.5 h / 8 - 72 °C

2.1: sodium / ethanol / 18 h / 20 - 70 °C

With sodium; trichlorophosphate; In ethanol;