2-(3-Hydroxypropyl)cyclohexanone

Base Information

Chemical Name:2-(3-Hydroxypropyl)cyclohexanone
CAS No.:62456-11-5
Molecular Formula:C₉H₁₆O₂
Molecular Weight:156.225
Hs Code.:
DSSTox Substance ID:DTXSID00482120
Nikkaji Number:J648.855B

Synonyms:2-(3-hydroxypropyl)cyclohexanone;2-(3-hydroxypropyl)cyclohexan-1-one;62456-11-5;Cyclohexanone, 2-(3-hydroxypropyl)-;SCHEMBL11595453;DTXSID00482120;AKOS015907259;2-(3-hydroxy-propyl)-cyclohexan-1-one;EN300-219321

Suppliers and Price of 2-(3-Hydroxypropyl)cyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(3-Hydroxypropyl)cyclohexanone

Chemical Property:

XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:156.115029749
Heavy Atom Count:11
Complexity:132

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=O)C(C1)CCCO

Technology Process of 2-(3-Hydroxypropyl)cyclohexanone

There total 4 articles about 2-(3-Hydroxypropyl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 503-30-0
trimethylene oxide

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 62456-11-5
2-(γ-Hydroxypropyl)-cyclohexanon

Guidance literature:: cyclohexanone; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

trimethylene oxide; With boron trifluoride diethyl etherate; In tetrahydrofuran; at -78 ℃; for 3h;
DOI:10.1002/anie.202012720

Reference yield:

: 2-[3-(Dimethyl-phenyl-silanyl)-propyl]-cyclohexanone

: 62456-11-5
2-(γ-Hydroxypropyl)-cyclohexanon

Guidance literature:: With tetrafluoroboric acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) Et₂O, CH₂Cl₂, r.t., 2 h, 2.) 6 h;
DOI:10.1021/jo00113a027

Reference yield:

: 94-66-6
2-allylcyclohexan-1-one

: 62456-11-5
2-(γ-Hydroxypropyl)-cyclohexanon

Guidance literature:: With sodium perborate; bis(cyclohexanyl)borane; Multistep reaction; 1.) THF, RT, 2 h, 2.) THF, RT, 2 h;
DOI:10.1139/v98-042