Technology Process of Undec-6-enoic acid
There total 4 articles about Undec-6-enoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
(5-carboxypentyl)triphenylphosphonium bromide;
With
sodium hexamethyldisilazane;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
Inert atmosphere;
pentanal;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
stereoselective reaction;
DOI:10.1016/j.bmc.2010.10.060
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid; hydrogen bromide / 7 h / 20 °C / Reflux
2.1: toluene / 48 h / Inert atmosphere; Reflux
3.1: sodium hexamethyldisilazane / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
3.2: 3 h / 20 °C
With
sulfuric acid; hydrogen bromide; sodium hexamethyldisilazane;
In
tetrahydrofuran; toluene;
3.2: Wittig reaction;
DOI:10.1016/j.bmc.2010.10.060
