3-methoxy-N-(4-nitrophenyl)benzamide

Base Information

Chemical Name:3-methoxy-N-(4-nitrophenyl)benzamide
CAS No.:62507-49-7
Molecular Formula:C14H12N2O4
Molecular Weight:272.26
Hs Code.:
DSSTox Substance ID:DTXSID50385450
Wikidata:Q82178247

Synonyms:3-methoxy-N-(4-nitrophenyl)benzamide;STK259264;62507-49-7;Cambridge id 5230876;Oprea1_219180;DTXSID50385450;AKOS001572601;CCG-316873;EU-0067406;SR-01000393881;SR-01000393881-1

Suppliers and Price of 3-methoxy-N-(4-nitrophenyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-methoxy-N-(4-nitrophenyl)benzamide

Chemical Property:

PSA：84.15000
LogP:3.45190
XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:272.07970687
Heavy Atom Count:20
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC(=C1)C(=O)NC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of 3-methoxy-N-(4-nitrophenyl)benzamide

There total 4 articles about 3-methoxy-N-(4-nitrophenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.2%

: C₈H₇ClO₃

: 100-01-6,104810-17-5
4-nitro-aniline

: 62507-49-7
3-methoxy-N-(4-nitrophenyl)benzamide

Guidance literature:: With triethylamine; In dichloromethane; at -20 - 20 ℃;

Reference yield:

: 1711-05-3
m-anisoyl chloride

: 100-01-6,104810-17-5
4-nitro-aniline

: 62507-49-7
3-methoxy-N-(4-nitrophenyl)benzamide

Guidance literature:: In 1,4-dioxane;

Reference yield:

: 586-38-9
3-Methoxybenzoic acid

: 62507-49-7
3-methoxy-N-(4-nitrophenyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 4 h / Reflux

2: triethylamine / dichloromethane / 0 - 20 °C

With thionyl chloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1248/cpb.c16-00154