Benzenesulfonamide, 4-methyl-N-[2-[[(4-methylphenyl)sulfonyl]oxy]-1-phenylethyl]-, (R)-

Base Information

Chemical Name:Benzenesulfonamide, 4-methyl-N-[2-[[(4-methylphenyl)sulfonyl]oxy]-1-phenylethyl]-, (R)-
CAS No.:62596-61-6
Molecular Formula:C22H23NO5S2
Molecular Weight:445.55200
Hs Code.:

Synonyms:(R)-1-Phenyl-1-(toluol-4-sulfonylamino)-2-(toluol-4-sulfonyloxy)-aethan;Toluene-4-sulfonic acid (R)-2-phenyl-2-(toluene-4-sulfonylamino)-ethyl ester;(R)-1-phenyl-1-(toluene-4-sulfonylamino)-2-(toluene-4-sulfonyloxy)-ethane;(R)-2-phenyl-O-(p-tolylsulfonyl)-2-<(p-tolylsulfonyl)amino>ethanol;

Suppliers and Price of Benzenesulfonamide, 4-methyl-N-[2-[[(4-methylphenyl)sulfonyl]oxy]-1-phenylethyl]-, (R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, 4-methyl-N-[2-[[(4-methylphenyl)sulfonyl]oxy]-1-phenylethyl]-, (R)-

Chemical Property:

PSA：106.30000
LogP:6.28100

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenesulfonamide, 4-methyl-N-[2-[[(4-methylphenyl)sulfonyl]oxy]-1-phenylethyl]-, (R)-

There total 1 articles about Benzenesulfonamide, 4-methyl-N-[2-[[(4-methylphenyl)sulfonyl]oxy]-1-phenylethyl]-, (R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 56613-80-0
D-2-phenylglycinol

: 98-59-9
p-toluenesulfonyl chloride

: 62596-61-6
(R)-2-phenyl-O-(p-tolylsulfonyl)-2-<(p-tolylsulfonyl)amino>ethanol

Guidance literature:: With pyridine; at 4 ℃; for 24h;

Reference yield: 89.0%

: 62596-61-6
(R)-2-phenyl-O-(p-tolylsulfonyl)-2-<(p-tolylsulfonyl)amino>ethanol

: 10387-40-3
potassium thioacetate

: 141089-96-5
(R)-S-acetyl-2-phenyl-2-<(p-tolylsulfonyl)amino>ethanethiol

Guidance literature:: In acetone; for 12h; Ambient temperature;

Reference yield:

: 62596-61-6
(R)-2-phenyl-O-(p-tolylsulfonyl)-2-<(p-tolylsulfonyl)amino>ethanol

: N-[(2S)-2-amino-2-phenylethyl]-4-methylbenzenesulfonamide

: N-((R)-2-amino-1-phenylethyl)-4-methylbenzenesulfonamide

Guidance literature:: (R)-2-phenyl-O-(p-tolylsulfonyl)-2-<(p-tolylsulfonyl)amino>ethanol; With sodium azide; In N,N-dimethyl-formamide; at 85 ℃; for 2.5h;

With hydrogen; palladium on activated charcoal; In ethanol; at 18 - 22 ℃;
DOI:10.1016/j.tetasy.2004.05.025