1-(4,4-diphenylbutyl)-4-methylpiperazine dihydrochloride

Base Information

Chemical Name:1-(4,4-diphenylbutyl)-4-methylpiperazine dihydrochloride
CAS No.:37028-02-7
Molecular Formula:C21H30Cl2N2
Molecular Weight:381.3823
Hs Code.:

Synonyms:

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4,4-diphenylbutyl)-4-methylpiperazine dihydrochloride

Chemical Property:

Vapor Pressure:7.67E-08mmHg at 25°C
Boiling Point:437.1°Cat760mmHg
Flash Point:195.8°C
Density:g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4,4-diphenylbutyl)-4-methylpiperazine dihydrochloride

There total 6 articles about 1-(4,4-diphenylbutyl)-4-methylpiperazine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 106002-98-6
4,4-Diphenylbutyric Acid, N-Methylpiperazinyl Amide Hydrochloride

: 37028-02-7
1-(4,4-Diphenyl-butyl)-4-methyl-piperazine; hydrochloride

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Ambient temperature;
DOI:10.1248/cpb.38.1570

Reference yield:

: 109-01-3
1-methyl-piperazine

: 37028-02-7
1-(4,4-Diphenyl-butyl)-4-methyl-piperazine; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1 h / Heating

2: 91 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1248/cpb.38.1570

Reference yield:

: 1008-76-0
4,5-dihydro-5-phenyl-2(3H)-furanone

: 37028-02-7
1-(4,4-Diphenyl-butyl)-4-methyl-piperazine; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / AlCl₃ / 5 h / Ambient temperature

2: triethylamine / CH₂Cl₂ / 1 h / 0 °C

3: 1 h / Heating

4: 91 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

With lithium aluminium tetrahydride; aluminium trichloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.38.1570