2-Propenoic acid,3-[2-[bis(2-chloroethyl)amino]phenyl]-,(4aS,4bR,6aS,8R,10aS,10bS,12aS)-octadecahydro-10a,12a-dimethyl-2-oxonaphtho[2,1-f]quinolin-8-ylester

Base Information

• Chemical Name: 2-Propenoic acid,3-[2-[bis(2-chloroethyl)amino]phenyl]-,(4aS,4bR,6aS,8R,10aS,10bS,12aS)-octadecahydro-10a,12a-dimethyl-2-oxonaphtho[2,1-f]quinolin-8-ylester
• CAS No.: 147151-60-8
• Molecular Formula: C₃₂H₄₄Cl₂N₂O₃
• Molecular Weight: 575.619

Synonyms:17a-Aza-D-homoandrostan-17-one,3-[[3-[2-[bis(2-chloroethyl)amino]phenyl]-1-oxo-2-propenyl]oxy]-, (3a,5a)-

Chemical Property of 2-Propenoic acid,3-[2-[bis(2-chloroethyl)amino]phenyl]-,(4aS,4bR,6aS,8R,10aS,10bS,12aS)-octadecahydro-10a,12a-dimethyl-2-oxonaphtho[2,1-f]quinolin-8-ylester

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Technology Process of 2-Propenoic acid,3-[2-[bis(2-chloroethyl)amino]phenyl]-,(4aS,4bR,6aS,8R,10aS,10bS,12aS)-octadecahydro-10a,12a-dimethyl-2-oxonaphtho[2,1-f]quinolin-8-ylester

There total 1 articles about 2-Propenoic acid,3-[2-[bis(2-chloroethyl)amino]phenyl]-,(4aS,4bR,6aS,8R,10aS,10bS,12aS)-octadecahydro-10a,12a-dimethyl-2-oxonaphtho[2,1-f]quinolin-8-ylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

3β-hydroxy-13α-amino-13,17-seco-5α-androstan-17-oic-13,17-lactam (39932-99-5) + ortho-cinnamic acid (64976-97-2) → 3-β-hydroxy-17a-aza-D-homo-5α-androstan-17-one ortho-cinnamate (137866-25-2,147151-60-8)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 144h; Ambient temperature;

DOI:10.1002/jps.2600820218

Reference yield:

3-β-hydroxy-17a-aza-D-homo-5α-androstan-17-one ortho-cinnamate (137866-25-2,147151-60-8) → 3-β-hydroxy-17a-aza-D-homo-5α-androstan-17-one p-cinnamate

Guidance literature:

With water; In acetonitrile; at 66 ℃;

DOI:10.1016/0223-5234(91)90203-Y

Reference yield:

3-β-hydroxy-17a-aza-D-homo-5α-androstan-17-one ortho-cinnamate (137866-25-2,147151-60-8) → 3-β-hydroxy-17a-aza-D-homo-5α-androstan-17-one m-cinnamate

Guidance literature:

With water; In acetonitrile; at 66 ℃;

DOI:10.1016/0223-5234(91)90203-Y

upstream raw materials:

3β-hydroxy-13α-amino-13,17-seco-5α-androstan-17-oic-13,17-lactam

ortho-cinnamic acid

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